{"id":17544,"date":"2018-07-28T01:00:00","date_gmt":"2018-08-08T00:59:24","guid":{"rendered":"http:\/\/www.05921.net\/index.php\/2018\/08\/08\/%e5%8a%a8%e5%9b%be%e8%a7%a3%e6%9e%90%e5%9b%9b%e5%a4%a7%e5%90%8d%e8%b0%b1%ef%bc%88ir%e3%80%81ms%e3%80%81nmr%e3%80%81uv%ef%bc%89%e5%b7%a5%e4%bd%9c%e5%8e%9f%e7%90%86\/"},"modified":"2018-08-08T08:59:30","modified_gmt":"2018-08-08T00:59:30","slug":"%e5%8a%a8%e5%9b%be%e8%a7%a3%e6%9e%90%e5%9b%9b%e5%a4%a7%e5%90%8d%e8%b0%b1%ef%bc%88ir%e3%80%81ms%e3%80%81nmr%e3%80%81uv%ef%bc%89%e5%b7%a5%e4%bd%9c%e5%8e%9f%e7%90%86","status":"publish","type":"post","link":"https:\/\/www.05921.net\/index.php\/17544\/","title":{"rendered":"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406"},"content":{"rendered":"
\n

\u70b9\u51fb\u4e0a\u65b9\u7684 \u884c\u821fDrug \u25b2 \u6dfb\u52a0\u5173\u6ce8<\/span><\/p>\n


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\u7ea2\u5916\u56fe\u8c31\uff08IR\uff09<\/span><\/p>\n<\/section>\n<\/section>\n<\/section>\n

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\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u4e9a\u7532\u57fa\u632f\u52a8\u6a21\u5f0f<\/span>
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\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u7532\u57fa\u632f\u52a8\u6a21\u5f0f<\/span><\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u7ea2\u5916\u5149\u8c31\u6d4b\u8bd5<\/span><\/p>\n


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<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

 \u7532\u9187\u7ea2\u5916\u5149\u8c31\u7ed3\u6784\u5206\u6790\u8fc7\u7a0b<\/span><\/p>\n


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\n
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\u7ea2\u5916\u5206\u6790\u53e3\u8bc0\uff1a<\/strong><\/span><\/section>\n<\/section>\n

<\/section>\n<\/section>\n<\/section>\n<\/section>\n


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\u6ed1\u52a8\u67e5\u770b\u66f4\u591a\u5185\u5bb9<\/span><\/p>\n

\n
\n

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1300\u6765\u5206\u754c\uff0c\u6ce8\u610f\u6a2a\u8f74\u5212\u5206\u5f02\u3002<\/span><\/p>\n

\u770b\u56fe\u8981\u77e5\u7ea2\u5916\u4eea\uff0c\u5f04\u6e05\u7269\u6001\u6db2\u56fa\u6c14\u3002<\/span><\/p>\n

\u6837\u54c1\u6765\u6e90\u5236\u6837\u6cd5\uff0c\u7269\u5316\u6027\u80fd\u591a\u8054\u7cfb\u3002<\/span><\/p>\n


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\u8bc6\u56fe\u5148\u5b66\u9971\u548c\u70c3\uff0c\u4e09\u5343\u4ee5\u4e0b\u770b\u5cf0\u5f62\u3002<\/span><\/p>\n

2960\u30012870\u662f\u7532\u57fa\uff0c2930\u30012850\u4e9a\u7532\u5cf0\u3002<\/span><\/p>\n

1470\u78b3\u6c22\u5f2f\uff0c1380\u7532\u57fa\u663e\u3002<\/span><\/p>\n

\u4e8c\u4e2a\u7532\u57fa\u540c\u4e00\u78b3\uff0c1380\u5206\u4e8c\u534a\u3002<\/span><\/p>\n

\u9762\u5185\u6447\u6446720\uff0c\u957f\u94fe\u4e9a\u7532\u4ea6\u53ef\u8fa8\u3002<\/span><\/p>\n


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\u672b\u7aef\u70ef\u70c3\u6b64\u5cf0\u5f3a\uff0c\u53ea\u6709\u4e00\u6c22\u4e0d\u660e\u663e\u3002<\/span><\/p>\n

\u5316\u5408\u7269\uff0c\u6709\u952e\u504f\uff0c\uff5e1650\u4f1a\u51fa\u73b0\u3002<\/span><\/p>\n

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910\u7aef\u57fa\u6c22\uff0c\u518d\u6709\u4e00\u6c22990\u3002<\/span><\/p>\n

\u987a\u5f0f\u4e8c\u6c22690\uff0c\u53cd\u5f0f\u79fb\u81f3970\uff1b<\/span><\/p>\n

\u5355\u6c22\u51fa\u5cf0820\uff0c\u5e72\u6270\u987a\u5f0f\u96be\u786e\u5b9a\u3002<\/span><\/p>\n


<\/p>\n

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\u4e09\u952e\u4f38\u5c55\u4e8c\u5343\u4e8c\uff0c\u7094\u6c22\u6447\u6446\u516d\u767e\u516b\u3002<\/span><\/p>\n


<\/p>\n

\u82b3\u70c3\u547c\u5438\u5f88\u7279\u5f81\uff0c1600\uff5e1430\u3002<\/span><\/p>\n

1650\uff5e2000\uff0c\u53d6\u4ee3\u65b9\u5f0f\u533a\u5206\u660e\u3002<\/span><\/p>\n

900\uff5e650\uff0c\u9762\u5916\u5f2f\u66f2\u5b9a\u82b3\u6c22\u3002<\/span><\/p>\n

\u4e94\u6c22\u5438\u6536\u6709\u4e24\u5cf0\uff0c700\u548c750\uff1b<\/span><\/p>\n

\u56db\u6c22\u53ea\u6709750\uff0c\u4e8c\u6c22\u76f8\u90bb830\uff1b<\/span><\/p>\n

\u95f4\u4e8c\u53d6\u4ee3\u51fa\u4e09\u5cf0\uff0c700\u3001780\uff0c880\u5904\u5b64\u7acb\u6c22<\/span><\/p>\n


<\/p>\n

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C\uff0dO\u4f38\u5c55\u5438\u6536\u5927\uff0c\u4f2f\u4ef2\u53d4\u9187\u4f4d\u4e0d\u540c\u3002<\/span><\/p>\n

1050\u4f2f\u9187\u663e\uff0c1100\u4e43\u662f\u4ef2\uff0c<\/span><\/p>\n

1150\u53d4\u9187\u5728\uff0c1230\u624d\u662f\u915a\u3002<\/span><\/p>\n


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1110\u919a\u94fe\u4f38\uff0c\u6ce8\u610f\u6392\u9664\u916f\u9178\u9187\u3002<\/span><\/p>\n

\u82e5\u4e0e\u03c0\u952e\u7d27\u76f8\u8fde\uff0c\u4e8c\u4e2a\u5438\u6536\u8981\u770b\u51c6\uff0c<\/span><\/p>\n

1050\u5bf9\u79f0\u5cf0\uff0c1250\u53cd\u5bf9\u79f0\u3002<\/span><\/p>\n

\u82ef\u73af\u82e5\u6709\u7532\u6c27\u57fa\uff0c\u78b3\u6c22\u4f38\u5c552820\u3002<\/span><\/p>\n

\u6b21\u7532\u57fa\u4e8c\u6c27\u8fde\u82ef\u73af\uff0c930\u5904\u6709\u5f3a\u5cf0\uff0c<\/span><\/p>\n

\u73af\u6c27\u4e59\u70f7\u6709\u4e09\u5cf0\uff0c1260\u73af\u632f\u52a8\uff0c<\/span><\/p>\n

\u4e5d\u767e\u4e0a\u4e0b\u53cd\u5bf9\u79f0\uff0c\u516b\u767e\u5de6\u53f3\u6700\u7279\u5f81\u3002<\/span><\/p>\n

\u7f29\u919b\u916e\uff0c\u7279\u6b8a\u919a\uff0c1110\u975e\u7f29\u916e\u3002<\/span><\/p>\n

\u9178\u9150\u4e5f\u6709C\uff0dO\u952e\uff0c\u5f00\u94fe\u73af\u9150\u6709\u533a\u522b\uff0c<\/span><\/p>\n

\u5f00\u94fe\u5f3a\u5bbd\u4e00\u5343\u4e00\uff0c\u73af\u9150\u79fb\u81f31250\u3002<\/span><\/p>\n


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\u7fb0\u57fa\u4f38\u5c55\u4e00\u5343\u4e03\uff0c2720\u5b9a\u919b\u57fa\u3002<\/span><\/p>\n

\u5438\u7535\u6548\u5e94\u6ce2\u6570\u9ad8\uff0c\u5171\u8f6d\u5219\u5411\u4f4e\u9891\u79fb\u3002<\/span><\/p>\n

\u5f20\u529b\u4fc3\u4f7f\u632f\u52a8\u5feb\uff0c\u73af\u5916\u53cc\u952e\u53ef\u7c7b\u6bd4\u3002<\/span><\/p>\n


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\u4e8c\u5343\u4e94\u5230\u4e09\u5343\u4e09\uff0c\u7fa7\u9178\u6c22\u952e\u5cf0\u5f62\u5bbd\uff0c<\/span><\/p>\n

920\uff0c\u949d\u5cf0\u663e\uff0c\u7fa7\u57fa\u53ef\u5b9a\u4e8c\u805a\u9178\u3001<\/span><\/p>\n


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\u9178\u9150\u5343\u516b\u6765\u5076\u5408\uff0c\u53cc\u5cf060\u4e25\u76f8\u9694\uff0c<\/span><\/p>\n

\u94fe\u72b6\u9178\u9150\u9ad8\u9891\u5f3a\uff0c\u73af\u72b6\u9178\u9150\u9ad8\u9891\u5f31\u3002<\/span><\/p>\n


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\u7fa7\u9178\u76d0\uff0c\u5076\u5408\u751f\uff0c\u7fb0\u57fa\u4f38\u7f29\u51fa\u53cc\u5cf0\uff0c<\/span><\/p>\n

1600\u53cd\u5bf9\u79f0\uff0c1400\u5bf9\u79f0\u5cf0\u3002<\/span><\/p>\n


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1740\u916f\u7fb0\u57fa\uff0c\u4f55\u9178\u53ef\u770b\u78b3\u6c27\u5c55\u3002<\/span><\/p>\n

1180\u7532\u9178\u916f\uff0c1190\u662f\u4e19\u9178\uff0c<\/span><\/p>\n

1220\u4e59\u9178\u916f\uff0c1250\u82b3\u9999\u9178\u3002<\/span><\/p>\n

1600\u5154\u8033\u5cf0\uff0c\u5e38\u4e3a\u90bb\u82ef\u4e8c\u7532\u9178\u3002<\/span><\/p>\n

\u6c2e\u6c22\u4f38\u5c55\u4e09\u5343\u56db\uff0c\u6bcf\u6c22\u4e00\u5cf0\u5f88\u5206\u660e\u3002<\/span><\/p>\n

\u7fb0\u57fa\u4f38\u5c55\u9170\u80faI\uff0c1660\u6709\u5f3a\u5cf0\uff1b<\/span><\/p>\n

N\uff0dH\u53d8\u5f62\u9170\u80faII\uff0c1600\u5206\u4f2f\u4ef2\u3002<\/span><\/p>\n

\u4f2f\u80fa\u9891\u9ad8\u6613\u91cd\u53e0\uff0c\u4ef2\u9170\u56fa\u60011550\uff1b<\/span><\/p>\n

\u78b3\u6c2e\u4f38\u5c55\u9170\u80faIII\uff0c1400\u5f3a\u5cf0\u663e\u3002<\/span><\/p>\n


<\/span><\/p>\n

\u80fa\u5c16\u5e38\u6709\u5e72\u6270\u89c1\uff0cN\uff0dH\u4f38\u5c55\u4e09\u5343\u4e09\uff0c<\/span><\/p>\n

\u53d4\u80fa\u65e0\u5cf0\u4ef2\u80fa\u5355\uff0c\u4f2f\u80fa\u53cc\u5cf0\u5c0f\u800c\u5c16\u3002<\/span><\/p>\n

1600\u78b3\u6c22\u5f2f\uff0c\u82b3\u9999\u4ef2\u80fa\u5343\u4e94\u504f\u3002<\/span><\/p>\n

\u516b\u767e\u5de6\u53f3\u9762\u5185\u6447\uff0c\u786e\u5b9a\u6700\u597d\u53d8\u6210\u76d0\u3002<\/span><\/p>\n

\u4f38\u5c55\u5f2f\u66f2\u4e92\u9760\u8fd1\uff0c\u4f2f\u80fa\u76d0\u4e09\u5343\u5f3a\u5cf0\u5bbd\uff0c<\/span><\/p>\n


<\/span><\/p>\n

\u4ef2\u80fa\u76d0\u3001\u53d4\u80fa\u76d0\uff0c2700\u4e0a\u4e0b\u53ef\u5206\u8fa8\uff0c<\/span><\/p>\n

\u4e9a\u80fa\u76d0\uff0c\u66f4\u53ef\u601c\uff0c2000\u5de6\u53f3\u624d\u53ef\u89c1\u3002<\/span><\/p>\n


<\/p>\n

\u785d\u57fa\u4f38\u7f29\u5438\u6536\u5927\uff0c\u76f8\u8fde\u57fa\u56e2\u53ef\u5f04\u6e05\u3002<\/span><\/p>\n

1350\u30011500\uff0c\u5206\u4e3a\u5bf9\u79f0\u53cd\u5bf9\u79f0\u3002<\/span><\/p>\n


<\/p>\n

\u6c28\u57fa\u9178\uff0c\u6210\u5185\u76d0\uff0c3100\uff5e2100\u5cf0\u5f62\u5bbd\u3002<\/span><\/p>\n

1600\u30011400\u9178\u6839\u5c55\uff0c1630\u30011510\u78b3\u6c22\u5f2f\u3002<\/span><\/p>\n

\u76d0\u9178\u76d0\uff0c\u7fa7\u57fa\u663e\uff0c\u94a0\u76d0\u86cb\u767d\u4e09\u5343\u4e09\u3002<\/span><\/p>\n


<\/p>\n

\u77ff\u7269\u7ec4\u6210\u6742\u800c\u4e71\uff0c\u632f\u52a8\u5149\u8c31\u8fdc\u7ea2\u7aef\u3002<\/span><\/p>\n

\u949d\u76d0\u7c7b\uff0c\u8f83\u7b80\u5355\uff0c\u5438\u6536\u5cf0\uff0c\u5c11\u800c\u5bbd\u3002<\/span><\/p>\n

\u6ce8\u610f\u7f9f\u57fa\u6c34\u548c\u94f5\uff0c\u5148\u8bb0\u51e0\u79cd\u666e\u901a\u76d0\u3002<\/span><\/p>\n

1100\u662f\u786b\u9178\u6839\uff0c1380\u785d\u9178\u76d0\uff0c<\/span><\/p>\n

1450\u78b3\u9178\u6839\uff0c\u4e00\u5343\u5de6\u53f3\u770b\u78f7\u9178\u3002<\/span><\/p>\n

\u7845\u9178\u76d0\uff0c\u4e00\u5cf0\u5bbd\uff0c1000\u771f\u58ee\u89c2\u3002<\/span><\/p>\n

\u52e4\u5b66\u82e6\u7ec3\u591a\u5b9e\u8df5\uff0c\u7ea2\u5916\u8bc6\u8c31\u4e0d\u7b97\u96be\u3002<\/span><\/p>\n<\/section>\n<\/section>\n

\n
\n
\n

\u8d28\u8c31\uff08MS\uff09<\/span><\/p>\n<\/section>\n<\/section>\n<\/section>\n


<\/span><\/p>\n

\u8d28\u8c31\u5206\u6790\u662f\u5148\u5c06\u7269\u8d28\u79bb\u5b50\u5316\uff0c\u6309\u79bb\u5b50\u7684\u8d28\u8377\u6bd4\u5206\u79bb\uff0c\u7136\u540e\u6d4b\u91cf\u5404\u79cd\u79bb\u5b50\u8c31\u5cf0\u7684\u5f3a\u5ea6\u800c\u5b9e\u73b0\u5206\u6790\u76ee\u7684\u7684\u4e00\u79cd\u5206\u6790\u65b9\u6cd5\u3002<\/span>\u8d28\u8c31\u5206\u6790\u539f\u7406<\/span><\/strong>\uff1a\u5206\u5b50\u5728\u771f\u7a7a\u4e2d\u88ab\u7535\u5b50\u8f70\u51fb\uff0c\u5f62\u6210\u79bb\u5b50\uff0c\u901a\u8fc7\u7535\u78c1\u573a\u6309\u4e0d\u540cm\/e\u5206\u79bb\uff1b<\/span>\u8c31\u56fe\u7684\u8868\u793a\u65b9\u6cd5<\/span><\/strong>\uff1a\u4ee5\u68d2\u56fe\u5f62\u5f0f\u8868\u793a\u79bb\u5b50\u7684\u76f8\u5bf9\u5cf0\u5ea6\u968fm\/e\u7684\u53d8\u5316\uff1b<\/span>\u63d0\u4f9b\u7684\u4fe1\u606f<\/span><\/strong>\uff1a\u5206\u5b50\u79bb\u5b50\u53ca\u788e\u7247\u79bb\u5b50\u7684\u8d28\u91cf\u6570\u53ca\u5176\u76f8\u5bf9\u5cf0\u5ea6\uff0c\u63d0\u4f9b\u5206\u5b50\u91cf\uff0c\u5143\u7d20\u7ec4\u6210\u53ca\u7ed3\u6784\u7684\u4fe1\u606f\uff0c\u53ef\u4ee5\u7528\u4e8e\u6d4b\u5b9a\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u3001\u5316\u5408\u7269\u5206\u5b50\u5f0f\u53ca\u7ed3\u6784\u5f0f\u3002<\/span><\/span><\/p>\n

<\/span><\/p>\n


<\/span><\/strong><\/p>\n

\u8d28\u8c31\u6837\u54c1\uff1a<\/span><\/span><\/strong>\u9002\u5408\u5206\u6790\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u4e3a50~2000 \u03bc\u7684\u6db2\u4f53\u3001\u56fa\u4f53\u6709\u673a\u5316\u5408\u7269\u6837\u54c1\uff0c\u8bd5\u6837\u5e94\u5c3d\u53ef\u80fd\u4e3a\u7eaf\u51c0\u7684\u5355\u4e00\u7ec4\u5206\u3002<\/span><\/span><\/p>\n


<\/span><\/p>\n

\u4ee5\u4e0b\u662fFT-ICR\u8d28\u8c31\u4eea\u5de5\u4f5c\u8fc7\u7a0b\uff1a<\/span><\/strong><\/span><\/p>\n

 <\/span><\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u79bb\u5b50\u4ea7\u751f<\/span><\/strong><\/p>\n


<\/span><\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u79bb\u5b50\u6536\u96c6<\/span><\/strong><\/p>\n


<\/span><\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u79bb\u5b50\u4f20\u8f93<\/span><\/strong><\/p>\n


<\/span><\/p>\n

FT-ICR\u8d28\u8c31\u7684\u5206\u6790\u5668\u662f\u4e00\u4e2a\u5177\u6709\u5747\u5300\uff08\u8d85\u5bfc\uff09\u78c1\u573a\u7684\u7a7a\u8154\uff0c<\/span>\u79bb\u5b50\u5728\u5782\u76f4\u4e8e\u78c1\u573a\u7684\u5706\u5f62\u8f68\u9053\u4e0a\u4f5c\u56de\u65cb\u8fd0\u52a8\uff0c\u56de\u65cb\u9891\u7387\u4ec5\u4e0e\u78c1\u573a\u5f3a\u5ea6\u548c\u79bb\u5b50\u7684\u8d28\u8377\u6bd4\u6709\u5173<\/span><\/strong>\uff0c\u56e0\u6b64\u53ef\u4ee5\u5206\u79bb\u4e0d\u540c\u8d28\u8377\u6bd4\u7684\u79bb\u5b50\uff0c\u5e76\u5f97\u5230\u8d28\u8377\u6bd4\u76f8\u5173\u7684\u56fe\u8c31\u3002<\/span><\/span><\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u79bb\u5b50\u56de\u65cb\u8fd0\u52a8<\/span><\/strong><\/span><\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u5085\u7acb\u53f6\u53d8\u6362<\/span><\/strong><\/span><\/p>\n


<\/p>\n

\n
\n
\n
\n
\u5e38\u89c1\u6709\u673a\u5316\u5408\u7269\u7684\u8d28\u8c31\uff1a<\/span><\/strong><\/span><\/section>\n<\/section>\n

<\/section>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

\u6ed1\u52a8\u67e5\u770b\u66f4\u591a\u5185\u5bb9<\/span><\/strong><\/p>\n

\n
\n

1. \u9971\u548c\u8102\u80aa\u70c3<\/span><\/strong><\/span><\/p>\n

a.\u76f4\u94fe\u70c3<\/span><\/strong><\/p>\n

\u76f4\u94fe\u70c3\u663e\u793a\u5f31\u7684\u5206\u5b50\u79bb\u5b50\u5cf0\uff0c<\/span><\/p>\n

\u25c6 \u6709m\/z \uff1aM-29\uff0c29\uff0c43\uff0c57\uff0c71\uff0c\u2026CnH2n\uff0b1\u7cfb\u5217\u5cf0(\u03c3\u2014\u65ad\u88c2)<\/span><\/p>\n

\u25c6  \u4f34\u6709m\/z \uff1a27\uff0c41\uff0c55\uff0c69\uff0c\u2026\u2026 CnH2n-1\u7cfb\u5217\u8f83\u5f31\u5cf0<\/span><\/p>\n


<\/span><\/strong><\/p>\n

b. \u652f\u94fe\u70c3<\/span><\/strong><\/p>\n

\u25c6\u5206\u5b50\u79bb\u5b50\u5cf0\u4e30\u5ea6\u964d\u4f4e<\/span>
<\/p>\n


<\/span><\/strong><\/p>\n

c. \u73af\u70f7\u70c3<\/span><\/strong><\/p>\n

\u25c6 \u5206\u5b50\u79bb\u5b50\u5cf0\u5f3a\u5ea6\u589e\u52a0\uff0c\u4f1a\u51fa\u73b0m\/z=41\uff0c55\uff0c56\uff0c69\u7b49\u7cfb\u5217\u788e\u7247\u79bb\u5b50\u5cf0\u3002<\/span>
<\/p>\n

\u25c6 \u70f7\u57fa\u53d6\u4ee3\u7684\u73af\u70f7\u70c3\u6613\u4e22\u5931\u70f7\u57fa\uff0c\u4f18\u5148\u5931\u53bb\u6700\u5927\u57fa\u56e2\uff0c\u6b63\u7535\u8377\u4fdd\u7559\u5728\u73af\u4e0a\u3002<\/span><\/p>\n


<\/span><\/p>\n

2.  \u70ef\u70c3<\/span><\/strong><\/span><\/p>\n

\u5bb9\u6613\u53d1\u751f\u70ef\u4e19\u57fa\u65ad\u88c2\uff0c<\/span><\/p>\n

\u4ea7\u751f\u4e00\u7cfb\u521727\uff0c41\uff0c55\uff0c69\uff0c\u2026CnH2n-1\u5cf0\uff0c41\u5e38\u662f\u57fa\u5cf0<\/span><\/p>\n

<\/span><\/p>\n


<\/span><\/p>\n

3. \u82b3\u70c3<\/span><\/strong><\/span><\/p>\n

\u5206\u5b50\u79bb\u5b50\u5cf0\u5f3a\uff0c\u6613\u53d1\u751fC\u03b1-C\u03b2\u952e\u7684\u88c2\u89e3\uff0c\u751f\u6210\u7684\u82c4\u57fam\/z91\u662f\u57fa\u5cf0\u3002\u6b63\u6784\u70f7\u57fa\u53d6\u4ee3\u94fe\u8d8a\u957f\uff0cm\/z91\u4e30\u5ea6\u8d8a\u5927\u3002<\/span><\/p>\n

\u82e5\u57fa\u5cf0\u6bd491\u592714n\uff0c\u8868\u660e\u82ef\u73af\u03b1\u78b3\u4e0a\u53e6\u6709\u70f7\u57fa\u53d6\u4ee3\u3002<\/span><\/p>\n

\u4f1a\u51fa\u73b039\uff0c51\uff0c65\uff0c77\uff0c91\uff0c105\uff0c119\uff0c\u2026\u7b49\u4e00\u7cfb\u5217\u5cf0\u3002<\/span><\/p>\n

\u4fa7\u94fe\u542b\u03b3-H\u7684\u4f1a\u4ea7\u751f\u91cd\u6392\u79bb\u5b50\u5cf0\uff0cm\/z=92          <\/span><\/p>\n


<\/span><\/p>\n

4. \u9187\u548c\u915a<\/span><\/strong><\/span><\/p>\n

\u9187\u7684\u5206\u5b50\u79bb\u5b50\u5cf0\u5f80\u5f80\u89c2\u5bdf\u4e0d\u5230\uff0cM-H\u6709\u65f6\u53ef\u4ee5\u89c2\u5bdf\u5230<\/span><\/p>\n

\u9971\u548c\u9187\u7f9f\u57fa\u7684C\u03b1\uff0dC\u03b2\u952e\u6613\u53d1\u751f\u65ad\u88c2\uff0c\u4ea7\u751f\uff0831+14n\uff09\u7279\u5f81\u7cfb\u5217\u79bb\u5b50\u5cf0\uff0c\u4f2f\u9187\u7684m\/z31\u8f83\u5f3a\u3002<\/span><\/p>\n

\u5f00\u94fe\u4f2f\u9187\u8fd8\u53ef\u80fd\u53d1\u751f\u9ea6\u6c0f\u91cd\u6392\uff0c\u540c\u65f6\u8131\u6c34\u548c\u8131\u70ef\uff08M-18-28\uff09\u3002<\/span><\/p>\n

\u915a\u7684\u5206\u5b50\u79bb\u5b50\u5cf0\u8f83\u5f3a\uff0c\u51fa\u73b0(M-28)\uff08-CO\uff09\uff0c(M-29)\uff08-CHO\uff09\u5cf0\u3002<\/span><\/p>\n


<\/span><\/p>\n

5. \u919b\u3001\u916e<\/span><\/strong><\/span><\/p>\n

\u76f4\u94fe\u919b\u3001\u916e\u663e\u793a\u6709CnH2n\uff0b1CO\u4e3a\u901a\u5f0f\u7684\u7279\u5f81\u79bb\u5b50\u7cfb\u5217\u5cf0\uff0c\u5982m\/z 29\u300143\u300157 \u2026\u2026\u7b49 \u3002<\/span><\/p>\n


<\/span><\/p>\n

6. \u7fa7\u9178<\/span><\/strong><\/span><\/p>\n

\u8102\u80aa\u7fa7\u9178\u7684\u5206\u5b50\u79bb\u5b50\u5cf0\u5f88\u5f31\uff0cm\/z  60\u662f\u4e01\u9178\u4ee5\u4e0a\u03b1\uff0d\u78b3\u539f\u5b50\u4e0a\u6ca1\u6709\u652f\u94fe\u7684\u8102\u80aa\u7fa7\u9178\u6700\u7279\u5f81\u7684\u79bb\u5b50\u5cf0\uff0c\u7531\u9ea6\u6c0f\u91cd\u6392\u88c2\u89e3\u4ea7\u751f \uff1b<\/span><\/p>\n

\u4f4e\u7ea7\u8102\u80aa\u9178\u8fd8\u5e38\u6709M\uff0d17\uff08\u5931\u53bbOH\uff09\u3001M\uff0d18\uff08\u5931\u53bbH2O\uff09\u3001M-45(\u5931\u53bbCO2H)\u7684\u79bb\u5b50\u5cf0\u3002<\/span><\/p>\n


<\/span><\/p>\n

7. \u916f<\/span><\/strong><\/span><\/p>\n

\u7fa7\u9178\u916f\u8fdb\u884c\u03b1\uff0d\u88c2\u89e3\u6240\u4ea7\u751f\uff08M-R\uff09\u6216\uff08M-OR\uff09\u7684\u79bb\u5b50\u5e38\u6210\u4e3a\u8d28\u8c31\u56fe\u4e2d\u7684\u5f3a\u5cf0\uff08\u6709\u65f6\u4e3a\u57fa\u5cf0\uff09\u3002<\/span><\/p>\n


<\/span><\/p>\n


<\/p>\n<\/section>\n<\/section>\n


<\/p>\n

\n
\n
\n

\u6838\u78c1\u5171\u632f\u8c31\uff08NMR\uff09<\/span><\/p>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

\u5728\u5916\u52a0\u78c1\u573a\u7684\u4f5c\u7528\u4e0b\uff0c\u81ea\u65cb\u6838\u5438\u6536\u7535\u78c1\u6ce2\u7684\u80fd\u91cf\u540e\u4ece\u4f4e\u81ea\u65cb\u80fd\u7ea7\u8dc3\u8fc1\u5230\u9ad8\u81ea\u65cb\u80fd\u7ea7\uff0c\u6240\u5f97\u5230\u7684\u7684\u5438\u6536\u56fe\u8c31\u4e3a\u6838\u78c1\u5171\u632f\u8c31\u3002<\/span>\u6838\u78c1\u5149\u8c31\u5206\u6790\u539f\u7406<\/span><\/strong>\uff1a\u5728\u5916\u78c1\u573a\u4e2d\uff0c\u5177\u6709\u6838\u78c1\u77e9\u7684\u539f\u5b50\u6838\uff0c\u5438\u6536\u5c04\u9891\u80fd\u91cf\uff0c\u4ea7\u751f\u6838\u81ea\u65cb\u80fd\u7ea7\u7684\u8dc3\u8fc1\uff1b<\/span>\u8c31\u56fe\u7684\u8868\u793a\u65b9\u6cd5<\/span><\/strong>\uff1a\u5438\u6536\u5149\u80fd\u91cf\u968f\u5316\u5b66\u4f4d\u79fb\u7684\u53d8\u5316\uff1b<\/span>\u63d0\u4f9b\u7684\u4fe1\u606f<\/span><\/strong>\uff1a\u5cf0\u7684\u5316\u5b66\u4f4d\u79fb\u3001\u5f3a\u5ea6\u3001\u88c2\u5206\u6570\u548c\u5076\u5408\u5e38\u6570\uff0c\u63d0\u4f9b\u6838\u7684\u6570\u76ee\u3001\u6240\u5904\u5316\u5b66\u73af\u5883\u548c\u51e0\u4f55\u6784\u578b\u7684\u4fe1\u606f\uff0c\u53ef\u7528\u4e8e\u7814\u7a76<\/span>\u5206\u5b50\u7ed3\u6784\u3001\u6784\u578b\u6784\u8c61\u3001\u5206\u5b50\u52a8\u6001<\/span><\/strong>\u7b49\u3002<\/span><\/span><\/p>\n

<\/span><\/p>\n


<\/span><\/strong><\/span><\/p>\n

\u6838\u78c1\u6837\u54c1\u8981\u6c42\uff1a<\/span><\/strong>1)\u3001\u9001\u68c0\u6837\u54c1\u7eaf\u5ea6\u4e00\u822c\u5e94>95% \uff0c\u65e0\u94c1\u5c51\u3001\u7070\u5c18\u3001\u6ee4\u7eb8\u6bdb\u7b49\u6742\u8d28\u3002\u4e00\u822c\u6709\u673a\u7269\u987b\u63d0\u4f9b\u7684\u6837\u54c1\u91cf\uff1a1H\u8c31>5mg\uff0c13C\u8c31>15mg\uff0c\u5bf9\u805a\u5408\u7269\u6240\u9700\u7684\u6837\u54c1\u91cf\u5e94\u9002\u5f53\u589e\u52a0\uff1b<\/span>2)\u3001\u672c\u4eea\u5668\u914d\u7f6e\u4ec5\u80fd\u8fdb\u884c\u6db2\u4f53\u6837\u54c1\u5206\u6790\uff0c\u8981\u6c42\u6837\u54c1\u5728\u67d0\u79cd\u6c18\u4ee3\u6eb6\u5242\u4e2d\u6709\u826f\u597d\u7684\u6eb6\u89e3\u6027\u80fd\uff0c\u9001\u6837\u8005\u5e94\u5148\u9009\u597d\u6240\u7528\u6eb6\u5242\u3002\u672c\u5ba4\u5e38\u5907\u7684\u6c18\u4ee3\u6eb6\u5242\u6709\u6c2f\u4eff\u3001\u91cd\u6c34\u3001\u7532\u9187\u3001\u4e19\u916e\u3001DMSO\u3001\u82ef\u3001\u90bb\u4e8c\u6c2f\u82ef\u3001\u4e59\u8148\u3001\u5421\u5576\u3001\u918b\u9178\u3001\u4e09\u6c1f\u4e59\u9178\uff1b3)\u3001\u8bf7\u9001\u6837\u8005\u5c3d\u91cf\u63d0\u4f9b\u6837\u54c1\u7684\u53ef\u80fd\u7ed3\u6784\u6216\u6765\u6e90\u3002\u5982\u6709\u7279\u6b8a\u8981\u6c42(\u5982\uff0c\u68c0\u6d4b\u6e29\u5ea6\u3001\u8c31\u5bbd\u7b49)\u8bf7\u4e8e\u8bf4\u660e\u3002<\/span><\/span><\/span><\/p>\n


<\/p>\n

\u4ee5\u4e0b\u662fNMR\u4eea\u5de5\u4f5c\u8fc7\u7a0b\uff08Bruker 950 US2\uff09\uff1a<\/span><\/strong><\/span><\/p>\n


<\/span><\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

NMR\u7ed3\u6784<\/span><\/strong><\/span><\/p>\n


<\/span><\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u8fdb\u6837<\/span><\/strong><\/span><\/p>\n


<\/span><\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u6837\u54c1\u5728\u78c1\u573a\u4e2d<\/span><\/strong><\/span><\/p>\n


<\/span><\/p>\n

\u5f53\u5916\u52a0\u5c04\u9891\u573a\u7684\u9891\u7387\u4e0e\u539f\u5b50\u6838\u81ea\u65cb\u8fdb\u52a8\u7684\u9891\u7387\u76f8\u540c\u65f6\uff0c\u5c04\u9891\u573a\u7684\u80fd\u91cf\u624d\u80fd\u88ab\u6709\u6548\u5730\u5438\u6536\uff0c\u56e0\u6b64\u5bf9\u4e8e\u7ed9\u5b9a\u7684\u539f\u5b50\u6838\uff0c<\/span>\u5728\u7ed9\u5b9a\u7684\u5916\u52a0\u78c1\u573a\u4e2d\uff0c\u53ea\u80fd\u5438\u6536\u7279\u5b9a\u9891\u7387\u5c04\u9891\u573a\u63d0\u4f9b\u7684\u80fd\u91cf\uff0c\u7531\u6b64\u5f62\u6210\u6838\u78c1\u5171\u632f\u4fe1\u53f7\u3002<\/span><\/strong><\/span><\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u6838\u78c1\u5171\u632f\u53ca\u6570\u636e\u8f93\u51fa<\/span><\/strong><\/span><\/p>\n


<\/p>\n

\n
\n
\n
\n
\u5e38\u89c1\u6c22\u8c31\u5316\u5b66\u4f4d\u79fb\u503c\u8303\u56f4\uff1a<\/span><\/strong><\/span><\/section>\n<\/section>\n

<\/section>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

\u6ed1\u52a8\u67e5\u770b\u66f4\u591a\u5185\u5bb9<\/span><\/strong><\/p>\n

\n
\n

\u919b\u6c229-10.5 ppm<\/span><\/p>\n

\u82b3\u73af\u53ca\u82ef\u73af6-9.5 ppm<\/span><\/p>\n

\u70ef\u6c224.5-7.5 ppm<\/span><\/p>\n

\u4e0e\u6c27\u539f\u5b50\u76f8\u8fde\u7684\u6c223.0-5.5ppm<\/span><\/p>\n

\u4e0e\u6c2e\u539f\u5b50\u76f8\u8fde\u7684\u6c222.0-3.5ppm<\/span><\/p>\n

\u7094\u6c221.6-3.4 ppm<\/span><\/p>\n

\u8102\u80aa\u6c220-2.5 ppm<\/span><\/p>\n

\u6d3b\u6cfc\u6c22\uff1a\u9187\u7c7b0.5-5.5ppm<\/span><\/p>\n

\u915a\u7c7b4.0-12.0 ppm<\/span><\/p>\n

\u9178\u7c7b\uff1a9-13.0 ppm<\/span><\/p>\n

\u6c28\u6d3b\u6cfc\u6c22\uff1a\u9170\u80fa5-8.5ppm<\/span><\/p>\n

\u82b3\u9999\u6c28 3.0-5.0ppm<\/span><\/p>\n

\u8102\u80aa\u6c280.6-3.5 ppm\u3002<\/span><\/p>\n


<\/p>\n<\/section>\n<\/section>\n


<\/span><\/strong><\/p>\n

\u78b3\u8c31\u4e09\u5927\u533a\uff1a<\/span><\/strong><\/p>\n

\u6ed1\u52a8\u67e5\u770b\u66f4\u591a\u5185\u5bb9<\/span><\/strong><\/span><\/p>\n

\n
\n

\u25c6  \u9ad8\u03b4\u503c\u533a\u03b4>165 ppm\uff0c\u5c5e\u4e8e\u7fb0\u57fa\u548c\u53e0\u70ef\u533a\uff1aa.\u5206\u5b50\u7ed3\u6784\u4e2d\uff0c\u5982\u5b58\u5728\u53e0\u5cf0\uff0c\u9664\u53e0\u70ef\u4e2d\u6709\u9ad8\u03b4\u503c\u4fe1\u53f7\u5cf0\u5916\uff0c\u53e0\u70ef\u4e24\u7aef\u78b3\u5728\u53cc\u952e\u533a\u57df\u8fd8\u5e94\u6709\u4fe1\u53f7\u5cf0\uff0c\u4e24\u79cd\u5cf0\u540c\u65f6\u5b58\u5728\u624d\u8bf4\u660e\u53e0\u70ef\u5b58\u5728\uff1bb.\u03b4>190 ppm\u7684\u4fe1\u53f7\uff0c\u53ea\u80fd\u5c5e\u4e8e\u919b\u3001\u916e\u7c7b\u5316\u5408\u7269\uff1bc.160-180 ppm\u7684\u4fe1\u53f7\u5cf0\uff0c\u5219\u5f52\u5c5e\u4e8e\u9178\u3001\u916f\u3001\u9178\u9150\u7b49\u7c7b\u5316\u5408\u7269\u7684\u7fb0\u57fa\u3002<\/span>
<\/p>\n

 <\/span><\/p>\n

\u25c6 \u4e2d\u03b4\u503c\u533a\u03b4 90-160 ppm\uff08\u4e00\u822c\u60c5\u51b5\u03b4\u4e3a100-150ppm\uff09\u70ef\u3001\u82b3\u73af\u3001\u9664\u53e0\u70ef\u4e2d\u592e\u78b3\u539f\u5b50\u5916\u7684\u5176\u4ed6SP2\u6742\u5316\u78b3\u539f\u5b50\u3001\u78b3\u6c2e\u4e09\u952e\u78b3\u539f\u5b50\u90fd\u5728\u8fd9\u4e2a\u533a\u57df\u51fa\u5cf0\u3002<\/span><\/p>\n

 <\/span><\/p>\n

\u25c6 \u4f4e\u03b4\u503c\u533a\u03b4<100 ppm\uff0c\u4e3b\u8981\u8102\u80aa\u94fe\u78b3\u539f\u5b50\u533a\uff1aa.\u4e0e\u5355\u4e2a\u6c27\u3001\u6c2e\u3001\u6c1f\u7b49\u6742\u539f\u5b50\u76f8\u8fde\u7684\u9971\u548c\u7684\u03b4\u503c\u4e00\u822c\u5904\u4e8e55-95 ppm\uff0c\u4e0d\u4e0e\u6c27\u3001\u6c2e\u3001\u6c1f\u7b49\u6742\u539f\u5b50\u76f8\u8fde\u7684\u9971\u548c\u7684\u03b4\u503c\u5c0f\u4e8e55 ppm\uff1bb.\u7094\u78b3\u539f\u5b50\u03b4\u503c\u572870-100ppm\uff0c\u8fd9\u662f\u4e0d\u9971\u548c\u78b3\u539f\u5b50\u7684\u7279\u4f8b\u3002<\/span><\/p>\n


<\/p>\n<\/section>\n<\/section>\n


<\/p>\n

\n
\n
\n

\u7d2b\u5916\u5149\u8c31\uff08UV\uff09<\/span><\/p>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

\u7269\u8d28\u5206\u5b50\u5438\u6536\u4e00\u5b9a\u7684\u6ce2\u957f\u7684\u7d2b\u5916\u5149\u65f6\uff0c\u5206\u5b50\u4e2d\u7684\u4ef7\u7535\u5b50\u4ece\u4f4e\u80fd\u7ea7\u8dc3\u8fc1\u5230\u9ad8\u80fd\u7ea7\u800c\u4ea7\u751f\u7684\u5438\u6536\u5149\u8c31\u8f83\u7d2b\u5916\u5149\u8c31\u3002<\/span>\u7d2b\u5916\u5438\u6536\u5149\u8c31\u5206\u6790\u539f\u7406\uff1a<\/strong><\/span>\u5438\u6536\u7d2b\u5916\u5149\u80fd\u91cf\uff0c\u5f15\u8d77\u5206\u5b50\u4e2d\u7535\u5b50\u80fd\u7ea7\u7684\u8dc3\u8fc1\uff1b<\/span>\u8c31\u56fe\u7684\u8868\u793a\u65b9\u6cd5\uff1a<\/span><\/strong>\u76f8\u5bf9\u5438\u6536\u5149\u80fd\u91cf\u968f\u5438\u6536\u5149\u6ce2\u957f\u7684\u53d8\u5316\uff1b<\/span>\u63d0\u4f9b\u7684\u4fe1\u606f\uff1a<\/span><\/strong>\u5438\u6536\u5cf0\u7684\u4f4d\u7f6e\u3001\u5f3a\u5ea6\u548c\u5f62\u72b6\uff0c\u63d0\u4f9b\u5206\u5b50\u4e2d\u4e0d\u540c\u7535\u5b50\u7ed3\u6784\u7684\u4fe1\u606f\uff0c\u4e3b\u8981\u7528\u4e8e\u6d4b\u5b9a\u5171\u8f6d\u5206\u5b50\u3001\u7ec4\u5206\u53ca\u5e73\u8861\u5e38\u6570\u3002<\/span><\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u5149\u7ebf\u4f20\u8f93<\/span><\/strong><\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"
<\/p>\n

\u5149\u884d\u5c04<\/strong><\/span><\/p>\n

<\/span><\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u63a2\u6d4b<\/span><\/strong><\/span><\/strong><\/span><\/p>\n


<\/p>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n

\u6570\u636e\u8f93\u51fa<\/span><\/strong><\/span><\/p>\n


<\/p>\n

\u7d2b\u5916\u5149\u8c31\u6837\u54c1\u8981\u6c42\uff1a1)\u3001\u6837\u54c1\u6eb6\u6db2\u7684\u6d53\u5ea6\u5fc5\u987b\u9002\u5f53\uff0c\u4e14\u5fc5\u987b\u6e05\u6f88\u900f\u660e\uff0c\u4e0d\u80fd\u6709\u6c14\u6ce1\u6216\u60ac\u6d6e\u7269\u8d28\u5b58\u5728\uff1b2)\u3001\u56fa\u4f53\u6837\u54c1\u91cf>0.2g\uff0c\u6db2\u4f53\u6837\u54c1\u91cf>2mL\u3002<\/span><\/p>\n


<\/span><\/p>\n

\n
\n
\n
\n
\u5e38\u89c1\u6709\u673a\u5316\u5408\u7269\u7684\u7d2b\u5916\u5438\u6536\u5149\u8c31<\/span><\/strong><\/section>\n<\/section>\n

<\/section>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

\u6ed1\u52a8\u67e5\u770b\u66f4\u591a\u5185\u5bb9<\/span><\/strong><\/p>\n

\n
\n

1.  \u9971\u548c\u70c3<\/span><\/strong>
<\/p>\n

\u9971\u548c\u5355\u952e\u78b3\u6c22\u5316\u5408\u7269\u53ea\u6709\u03c3\u7535\u5b50\uff0c\u56e0\u800c\u53ea\u80fd\u4ea7\u751f\u03c3\u2192\u03c3*\u8dc3\u8fc1\u3002\u7531\u4e8e\u03c3\u7535\u5b50\u6700\u4e0d\u5bb9\u6613\u6fc0\u53d1\uff0c\u9700\u8981\u5438\u6536\u5f88\u5927\u7684\u80fd\u91cf\uff0c\u624d\u80fd\u4ea7\u751f\u03c3\u2192\u03c3*\u8dc3\u8fc1\uff0c\u56e0\u800c\u8fd9\u7c7b\u5316\u5408\u7269\u5728200nm\u4ee5\u4e0a\u65e0\u5438\u6536\u3002\u6240\u4ee5\u5b83\u4eec\u5728\u7d2b\u5916\u5149\u8c31\u5206\u6790\u4e2d\u5e38\u7528\u4f5c\u6eb6\u5242\u4f7f\u7528\uff0c\u5982\u6b63\u5df2\u70f7\u3001\u73af\u4e59\u70f7\u3001\u5e9a\u70f7\u7b49\u3002<\/span><\/p>\n


<\/p>\n<\/section>\n<\/section>\n

\n
\n

\u7248\u6743\u58f0\u660e<\/span><\/strong><\/span><\/p>\n<\/section>\n<\/section>\n

\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n


<\/p>\n

\n
\n
\n
\n

\u6587\u7ae0\u4fe1\u606f\u6e90<\/span>\u4e8e\u516c<\/span>\u4f17\u53f7\u4e8c\u77e5\u4e86<\/span>\uff0c<\/span>\u767b\u8f7d\u8be5\u6587\u7ae0\u76ee\u7684\u4e3a\u66f4\u5e7f\u6cdb\u7684\u4f20\u9012\u884c\u4e1a\u4fe1\u606f\uff0c\u4e0d\u4ee3\u8868\u8d5e\u540c\u5176\u89c2\u70b9\u6216\u5bf9\u5176\u771f\u5b9e\u6027\u8d1f\u8d23\u3002\u6587\u7ae0\u7248\u6743\u5f52\u539f\u4f5c\u8005\u53ca\u539f\u51fa\u5904\u6240\u6709\uff0c\u6587\u7ae0\u5185\u5bb9\u4ec5\u4f9b\u53c2\u8003\u3002\u672c\u7f51\u62e5\u6709\u5bf9\u6b64\u58f0\u660e\u7684\u6700\u7ec8\u89e3\u91ca\u6743\uff0c\u82e5\u65e0\u610f\u4fb5\u72af\u7248\u6743\uff0c\u8bf7\u8054\u7cfb\u5c0f\u7f16\u5220\u9664\u3002<\/span><\/p>\n<\/section>\n<\/section>\n<\/section>\n

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\u5b66\u5982\u9006\u6c34\u884c\u821f\uff0c\u4e0d\u8fdb\u5219\u9000\uff1b<\/span><\/p>\n

\u5fc3\u4f3c\u5e73\u539f\u8d70\u9a6c\uff0c\u6613\u653e\u96be\u6536\u3002<\/span><\/p>\n<\/section>\n<\/section>\n<\/section>\n

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\"\u52a8\u56fe\u89e3\u6790\u56db\u5927\u540d\u8c31\uff08IR\u3001MS\u3001NMR\u3001UV\uff09\u5de5\u4f5c\u539f\u7406\"<\/p>\n<\/section>\n


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\u533b\u836f\u5927\u6570\u636e|\u884c\u4e1a\u52a8\u6001|\u653f\u7b56\u89e3\u8bfb<\/span><\/p>\n


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\u59cb\u53d1\u4e8e\u5fae\u4fe1\u516c\u4f17\u53f7\uff1a \u884c\u821fDrug <\/p>\n<\/blockquote>\n<\/div>\n","protected":false},"excerpt":{"rendered":"

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