{"id":30439,"date":"2018-08-07T01:00:00","date_gmt":"2018-08-09T04:08:52","guid":{"rendered":"http:\/\/www.05921.net\/index.php\/2018\/08\/09\/%e6%94%b6%e8%97%8f-hplc%e5%8f%b2%e4%b8%8a%e6%9c%80%e5%85%a8%e8%a7%a3%e6%9e%90-%e7%bb%9d%e5%af%b9%e5%ae%9e%e7%94%a8%e3%80%82%e3%80%82%e3%80%82\/"},"modified":"2018-08-09T12:08:53","modified_gmt":"2018-08-09T04:08:53","slug":"%e6%94%b6%e8%97%8f-hplc%e5%8f%b2%e4%b8%8a%e6%9c%80%e5%85%a8%e8%a7%a3%e6%9e%90-%e7%bb%9d%e5%af%b9%e5%ae%9e%e7%94%a8%e3%80%82%e3%80%82%e3%80%82","status":"publish","type":"post","link":"https:\/\/www.05921.net\/index.php\/30439\/","title":{"rendered":"\u6536\u85cf | HPLC\u53f2\u4e0a\u6700\u5168\u89e3\u6790\u2014\u2014\u7edd\u5bf9\u5b9e\u7528\u3002\u3002\u3002"},"content":{"rendered":"
\n

\"\u6536\u85cf<\/span><\/a><\/p>\n

\n
\n
\n

\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\u6cd5\uff1a\u4ee5\u6c14\u76f8\u8272\u8c31\u4e3a\u57fa\u7840\uff0c\u5728\u7ecf\u5178\u6db2\u76f8\u8272\u8c31\u5b9e\u9a8c\u548c\u6280\u672f\u57fa\u7840\u4e0a\u5efa\u7acb\u7684\u4e00\u79cd\u6db2\u76f8\u8272\u8c31\u6cd5\u3002\u3002\u3002<\/strong><\/p>\n<\/section>\n

<\/section>\n<\/section>\n<\/section>\n
\n
\n
\n

<\/section>\n
\n

HPLC\u4e0e\u7ecf\u5178LC\u533a\u522b<\/span><\/strong><\/span><\/p>\n<\/section>\n

\n
<\/section>\n
<\/section>\n<\/section>\n<\/section>\n
\n
<\/section>\n
<\/section>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

\u4e3b\u8981\u533a\u522b\uff1a<\/span><\/strong><\/span><\/p>\n

\u56fa\u5b9a\u76f8\u5dee\u522b\uff0c\u8f93\u6db2\u8bbe\u5907\u548c\u68c0\u6d4b\u624b\u6bb5\u3002<\/span><\/span><\/p>\n

1.LC\uff1a<\/span><\/strong>\u4ec5\u4f5c\u4e3a\u4e00\u79cd\u5206\u79bb\u624b\u6bb5\uff1b<\/span><\/span><\/p>\n

\u2460\u67f1\u5185\u5f841~3cm\uff0c\u56fa\u5b9a\u76f8\u7c92\u5f84>100\u03bcm\u4e14\u4e0d\u5747\u5300\uff1b<\/span><\/p>\n

\u2461\u5e38\u538b\u8f93\u9001\u6d41\u52a8\u76f8\uff1b<\/span><\/p>\n

\u2462\u67f1\u6548\u4f4e\uff08H\u2191\uff0cn\u2193\uff09\uff1b<\/span><\/p>\n

\u2463\u5206\u6790\u5468\u671f\u957f\uff1b<\/span><\/p>\n

\u2464\u65e0\u6cd5\u5728\u7ebf\u68c0\u6d4b\uff1b<\/span><\/p>\n

2.HPLC\uff1a<\/span><\/strong>\u5206\u79bb\u548c\u5206\u6790\uff1b<\/span><\/span><\/p>\n

\u2460\u67f1\u5185\u5f842~6mm\uff0c\u56fa\u5b9a\u76f8\u7c92\u5f84<10\u03bcm\uff08\u7403\u5f62\uff0c\u5300\u6d46\u88c5\u67f1\uff09\uff1b<\/span><\/p>\n

\u2461\u9ad8\u538b\u8f93\u9001\u6d41\u52a8\u76f8\uff1b<\/span><\/p>\n

\u2462\u67f1\u6548\u9ad8\uff08H\u2193\uff0cn\u2191\uff09\uff1b<\/span><\/p>\n

\u2463\u5206\u6790\u65f6\u95f4\u5927\u5927\u7f29\u77ed\uff1b    <\/span><\/p>\n

\u2464\u53ef\u4ee5\u5728\u7ebf\u68c0\u6d4b\uff1b<\/span><\/p>\n


<\/p>\n

\n
\n
\n
\n

HPLC\u4e0eGC\u5dee\u522b<\/span><\/strong><\/p>\n<\/section>\n

\n
<\/section>\n
<\/section>\n<\/section>\n<\/section>\n
\n
<\/section>\n
<\/section>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

\u76f8\u540c\uff1a<\/span><\/strong><\/span><\/p>\n

\u517c\u5177\u5206\u79bb\u548c\u5206\u6790\u529f\u80fd\uff0c\u5747\u53ef\u4ee5\u5728\u7ebf\u68c0\u6d4b\uff1b<\/span><\/p>\n

\u4e3b\u8981\u5dee\u522b\uff1a<\/span><\/strong><\/span><\/p>\n

\u5206\u6790\u5bf9\u8c61\u7684\u5dee\u522b\u548c\u6d41\u52a8\u76f8\u7684\u5dee\u522b\uff1b<\/span><\/p>\n

1.\u5206\u6790\u5bf9\u8c61<\/span><\/strong><\/span><\/p>\n

GC\uff1a<\/span><\/strong><\/span><\/p>\n

\u2460\u80fd\u6c14\u5316\u3001\u70ed\u7a33\u5b9a\u6027\u597d\u3001\u4e14\u6cb8\u70b9\u8f83\u4f4e\u7684\u6837\u54c1\uff1b<\/span><\/p>\n

\u2461\u9ad8\u6cb8\u70b9\u3001\u6325\u53d1\u6027\u5dee\u3001\u70ed\u7a33\u5b9a\u6027\u5dee\u3001\u79bb\u5b50\u578b\u53ca\u9ad8\u805a\u7269\u7684\u6837\u54c1\u4e0d\u53ef\u68c0\u6d4b\uff0c\u5360\u6709\u673a\u7269\u768420%\uff1b<\/span><\/p>\n

HPLC\uff1a<\/span><\/strong><\/span><\/p>\n

\u2460\u6eb6\u89e3\u540e\u80fd\u5236\u6210\u6eb6\u6db2\u7684\u6837\u54c1\uff1b<\/span><\/p>\n

\u2461\u4e0d\u53d7\u6837\u54c1\u6325\u53d1\u6027\u548c\u70ed\u7a33\u5b9a\u6027\u7684\u9650\u5236\uff1b<\/span><\/p>\n

\u2462\u5206\u5b50\u91cf\u5927\u3001\u96be\u6c14\u5316\u3001\u70ed\u7a33\u5b9a\u6027\u5dee\u53ca\u9ad8\u5206\u5b50\uff1b<\/span><\/p>\n

\u2463\u548c\u79bb\u5b50\u578b\u6837\u54c1\u5747\u53ef\u68c0\u6d4b\uff1b<\/span><\/p>\n

\u2464\u7528\u9014\u5e7f\u6cdb\uff0c\u5360\u6709\u673a\u7269\u768480%\uff1b<\/span><\/p>\n

2.\u6d41\u52a8\u76f8\u5dee\u522b<\/span><\/strong><\/span><\/p>\n

GC\uff1a<\/span><\/strong><\/span><\/p>\n

\u2460\u6d41\u52a8\u76f8\u4e3a\u60f0\u6027\u6c14\u4f53\uff1b<\/span><\/p>\n

\u2461\u7ec4\u5206\u4e0e\u6d41\u52a8\u76f8\u65e0\u4eb2\u5408\u4f5c\u7528\u529b\uff0c\u53ea\u4e0e\u56fa\u5b9a\u76f8\u4f5c\u7528\uff1b<\/span><\/p>\n

HPLC\uff1a<\/span><\/strong><\/span><\/p>\n

\u2460\u6d41\u52a8\u76f8\u4e3a\u6db2\u4f53\uff1b<\/span><\/p>\n

\u2461\u6d41\u52a8\u76f8\u4e0e\u7ec4\u5206\u95f4\u6709\u4eb2\u5408\u4f5c\u7528\u529b\uff0c\u4e3a\u63d0\u9ad8\u67f1\u7684\u9009\u62e9\u6027\u3001\u6539\u5584\u5206\u79bb\u5ea6\u589e\u52a0\u4e86\u56e0\u7d20\uff0c\u5bf9\u5206\u79bb\u8d77\u5f88\u5927\u4f5c\u7528\uff1b<\/span><\/p>\n

\u2462\u6d41\u52a8\u76f8\u79cd\u7c7b\u8f83\u591a\uff0c\u9009\u62e9\u4f59\u5730\u5e7f\uff1b<\/span><\/p>\n

\u2463\u6d41\u52a8\u76f8\u6781\u6027\u548cpH\u503c\u7684\u9009\u62e9\u4e5f\u5bf9\u5206\u79bb\u8d77\u5230\u91cd\u8981\u4f5c\u7528\uff1b<\/span><\/p>\n

\u2464\u9009\u7528\u4e0d\u540c\u6bd4\u4f8b\u7684\u4e24\u79cd\u6216\u4e24\u79cd\u4ee5\u4e0a\u6db2\u4f53\u4f5c\u4e3a\u6d41\u52a8\u76f8\uff1b<\/span><\/p>\n

\u2465\u53ef\u4ee5\u589e\u5927\u5206\u79bb\u9009\u62e9\u6027\uff1b<\/span><\/p>\n

3.\u64cd\u4f5c\u6761\u4ef6\u5dee\u522b<\/span><\/strong><\/span><\/p>\n

GC\uff1a<\/span><\/strong><\/span><\/p>\n

\u52a0\u6e29\u64cd\u4f5c<\/span>\uff1b
<\/span><\/span><\/p>\n

HPLC\uff1a<\/span><\/strong><\/span><\/p>\n

\u2460\u5ba4\u6e29\uff1b<\/span><\/p>\n

\u2461\u9ad8\u538b\uff1b\uff08\u7c98\u5ea6\u5927\uff0c\u5cf0\u5c55\u5bbd\u5c0f\uff09<\/strong><\/span><\/p>\n


<\/p>\n

\n
\n
\n
\n
HPLC\u6cd5\u4e2d\u5206\u79bb\u6761\u4ef6\u7684\u9009\u62e9<\/span><\/strong><\/section>\n<\/section>\n
\n
<\/section>\n
<\/section>\n<\/section>\n<\/section>\n
\n
<\/section>\n
<\/section>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

1.\u56fa\u5b9a\u76f8\u4e0e\u88c5\u67f1\u65b9\u6cd5\u7684\u9009\u62e9\uff1a<\/span><\/strong><\/span><\/p>\n

\u9009\u7c92\u5f84\u5c0f\u7684\u3001\u5206\u5e03\u5747\u5300\u7684\u7403\u5f62\u56fa\u5b9a\u76f8\uff08dp\u226410\u03bcm\uff09\uff1b<\/span><\/p>\n

\u9996\u9009\u5316\u5b66\u952e\u5408\u76f8\uff0c\u5300\u6d46\u6cd5\u88c5\u67f1\uff1b<\/span><\/p>\n

2.\u6d41\u52a8\u76f8\u53ca\u5176\u6d41\u901f\u7684\u9009\u62e9\uff1a<\/span><\/strong><\/span><\/p>\n

\u9009\u7c98\u5ea6\u5c0f\u3001\u4f4e\u6d41\u901f\u7684\u6d41\u52a8\u76f8\u2014\u7532\u9187\uff0c1mL\/min\uff1b<\/span><\/p>\n

3.\u67f1\u6e29\u7684\u9009\u62e9\uff1a<\/span><\/strong><\/span><\/p>\n

\u9009\u5ba4\u6e2925\u2103\u5de6\u53f3\uff1b<\/span><\/p>\n

\n
\n
\n
\n
\n
\u5404\u7c7b\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\u6cd5 <\/span><\/strong><\/section>\n<\/section>\n<\/section>\n
\n
<\/section>\n
<\/section>\n<\/section>\n<\/section>\n
\n
<\/section>\n
<\/section>\n<\/section>\n<\/section>\n<\/section>\n


<\/p>\n

(<\/span><\/strong>\u4e00<\/span>)<\/span>\u6db2\u56fa\u5438\u9644\u8272\u8c31\u6cd5\uff08<\/span>LSC<\/span>\uff09<\/span>      <\/span><\/span><\/strong><\/span><\/span><\/p>\n

 <\/span>\u6d41\u52a8\u76f8\u4e3a\u6db2\u4f53\uff0c\u56fa\u5b9a\u76f8\u4e3a\u56fa\u4f53\u5438\u9644\u5242<\/span>\uff1b<\/span>
<\/span>1<\/span>\uff0e\u5206\u79bb\u673a\u5236\uff1a<\/span><\/strong><\/span><\/p>\n

\u5229\u7528\u6eb6\u8d28\u5206\u5b50\u5360\u636e\u56fa\u5b9a\u76f8\u8868\u9762\u5438\u9644\u6d3b\u6027\u4e2d\u5fc3\u80fd\u529b\u5dee\u5f02\uff1b<\/span> 
<\/span>\u5206\u79bb\u524d\u63d0\uff1a<\/span><\/span><\/p>\n

K<\/span>\u4e0d\u7b49\u6216<\/span>k<\/span>\u4e0d\u7b49\uff1b<\/span>
<\/span>2<\/span>\uff0e\u56fa\u5b9a\u76f8\uff1a<\/span><\/strong><\/span><\/p>\n

\u4e0e<\/span>LC<\/span>\u6bd4\uff0c\u56fa\u5b9a\u76f8\u7c92\u5f84\u4e0d\u540c\uff08<\/span><10\u03bcm<\/span>\uff09\uff1b<\/span> 
<\/span>3<\/span>\uff0e\u6d41\u52a8\u76f8\uff1a<\/span><\/strong><\/span><\/p>\n

\u5e95\u5242\uff08\u70f7\u70c3\uff09<\/span>+<\/span>\u6709\u673a\u6781\u6027\u8c03\u8282\u5242\uff1b<\/span>   
<\/span>\u203b\u4f8b\uff1a\u6b63\u5df1\u70f7\u6216\u5e9a\u70f7<\/span>+<\/span>\u6c2f\u4eff\u3002\u3002\u3002<\/span><\/strong>
<\/span>4<\/span>\uff0e\u5f71\u54cd<\/span>K<\/span>\u7684\u56e0\u7d20\uff1a<\/span><\/strong><\/span><\/p>\n

\u4e0e\u56fa\u5b9a\u76f8\u6027\u8d28\u548c\u6d41\u52a8\u76f8\u6027\u8d28\u6709\u5173\uff1b<\/span>
<\/span>\u6eb6\u8d28\u5206\u5b50\u6781\u6027<\/span>\u2191<\/span>\uff0c\u6d17\u8131\u80fd\u529b<\/span>\u2193<\/span>\uff0c<\/span>k\u2191<\/span>\uff0c<\/span>tR<\/sub>\u2191<\/span>\uff1b<\/span>
<\/span>\u6eb6\u5242\u7cfb\u7edf\u6781\u6027<\/span>\u2191<\/span>\uff0c\u6d17\u8131\u80fd\u529b<\/span>\u2191<\/span>\uff0c<\/span>k\u2193<\/span>\uff0c<\/span>tR<\/sub>\u2193<\/span>\uff1b<\/span>
<\/span>\u6ce8\uff1a\u8c03\u8282\u6eb6\u5242\u6781\u6027\uff0c\u53ef\u4ee5\u63a7\u5236\u7ec4\u5206\u7684\u4fdd\u7559\u65f6\u95f4\uff1b<\/span><\/strong>
<\/span>5<\/span>\uff0e\u51fa\u67f1\u987a\u5e8f\uff1a<\/span><\/strong><\/span><\/p>\n

\u5f3a\u6781\u6027\u7ec4\u5206\u540e\u51fa\u67f1\uff0c\u5f31\u6781\u6027\u7ec4\u5206\u5148\u51fa\u67f1\uff1b<\/span>
<\/span>6<\/span>\uff0e\u7845\u80f6\u5438\u6c34\u91cf<\/span>\u2191<\/span>\uff0c<\/span>LSC\u2192LLC<\/span><\/strong>
<\/span>\u7845\u80f6\u542b\u6c34\u91cf\u8f83\u5c0f\uff0c\u5438\u9644\u8272\u8c31\uff0c\u7845\u80f6\u6781\u6027\u8f83\u5927\uff1b<\/span>
<\/span>\u7845\u80f6\u542b\u6c34\u91cf<\/span>>17% <\/span>\uff0c\u5206\u914d\u8272\u8c31\uff0c\u7845\u80f6\u5931\u6d3b<\/span>\u2192<\/span>\u8f7d\u4f53\uff1b<\/span>
<\/span>\u5438\u9644\u7684\u6c34<\/span>\u2192<\/span>\u56fa\u5b9a\u6db2<\/span><\/strong>
<\/span>(<\/span>\u4e8c<\/span>)<\/span>\u6db2<\/span>–<\/span>\u6db2\u5206\u914d\u8272\u8c31\u6cd5\uff08<\/span>LLC<\/span>\uff09<\/span><\/strong>
<\/span>1<\/span>\uff0e\u5206\u79bb\u673a\u5236\uff1a<\/span><\/strong><\/span><\/p>\n

\u5229\u7528\u7ec4\u5206\u5728\u4e24\u76f8\u4e2d\u6eb6\u89e3\u5ea6\u7684\u5dee\u5f02<\/span>
<\/span>2<\/span>\uff0e\u56fa\u5b9a\u76f8\uff1a<\/span><\/strong><\/span><\/p>\n

\u8f7d\u4f53<\/span>+<\/span>\u56fa\u5b9a\u6db2\uff08\u7269\u7406\u6216\u673a\u68b0\u6d82\u6e0d\u6cd5\uff09<\/strong><\/span>
<\/span>\u7f3a\u70b9\uff1a<\/span><\/strong><\/span><\/p>\n

\u7cfb\u7edf\u5185\u90e8\u538b\u529b\u5927\uff0c\u6613\u6d41\u5931\uff0c\u4e0d\u5b9e\u7528<\/span>
<\/span>\u56fa\u5b9a\u6db2<\/span>–<\/span>\u6781\u6027<\/span>\u2192NLLC<\/span><\/span><\/p>\n

\u56fa\u5b9a\u6db2<\/span>–<\/span>\u975e\u6781\u6027<\/span>\u2192RLLC
3.<\/span>\u2460\u6b63\u76f8\u8272\u8c31<\/span>–<\/span>\u56fa\u5b9a\u6db2\u6781\u6027<\/span>><\/span>\u6d41\u52a8\u76f8\u6781\u6027\uff08<\/span>NLLC<\/span>\uff09<\/span><\/strong>
<\/span>\u6781\u6027\u5c0f\u7684\u7ec4\u5206\u5148\u51fa\u67f1\uff0c\u6781\u6027\u5927\u7684\u7ec4\u5206\u540e\u51fa\u67f1\uff1a\u9002\u4e8e\u5206\u79bb\u6781\u6027\u7ec4\u5206\uff1b<\/span>
<\/span>\u2461\u53cd\u76f8\u8272\u8c31<\/span>–<\/span>\u56fa\u5b9a\u6db2\u6781\u6027<\/span><<\/span>\u6d41\u52a8\u76f8\u6781\u6027\uff08<\/span>RLLC<\/span>\uff09<\/span><\/strong><\/span><\/p>\n

\u6781\u6027\u5927\u7684\u7ec4\u5206\u5148\u51fa\u67f1\uff0c\u6781\u6027\u5c0f\u7684\u7ec4\u5206\u540e\u51fa\u67f1\uff1a\u9002\u4e8e\u5206\u79bb\u975e\u6781\u6027\u7ec4\u5206\uff1b<\/span>
<\/span>(<\/span>\u4e09<\/span>)<\/span>\u5316\u5b66\u952e\u5408\u76f8\u8272\u8c31\u6cd5\uff08<\/span>BPC<\/span>\uff09<\/span><\/strong>
<\/span>1.\u5316\u5b66\u952e\u5408\u76f8<\/span> <\/strong>
<\/span>\uff081\uff09<\/span>\u5206\u79bb\u673a\u5236\uff1a<\/span><\/strong><\/span><\/p>\n

\u5206\u914d<\/span>+<\/span>\u5438\u9644\uff08\u4ee5<\/span>LLC<\/span>\u4e3a\u57fa\u7840\uff09\uff1b<\/span>
<\/span>\uff082\uff09<\/span>\u7279\u70b9\uff1a<\/span><\/strong>
 1<\/span>\uff09\u4e0d\u6613\u6d41\u5931\uff1b<\/span>
 2<\/span>\uff09\u70ed\u7a33\u5b9a\u6027\u597d\uff1b<\/span>
 3<\/span>\uff09\u5316\u5b66\u6027\u80fd\u597d\uff1b<\/span>
 4<\/span>\uff09\u8f7d\u6837\u91cf\u5927\uff1b<\/span>
 5<\/span>\uff09\u9002\u4e8e\u68af\u5ea6\u6d17\u8131\uff1b<\/span>
<\/span>2.\u53cd\u76f8\u952e\u5408\u76f8\u8272\u8c31<\/span><\/strong>
<\/span>\uff081\uff09<\/span>\u5206\u79bb\u673a\u5236\uff1a<\/span><\/strong><\/span><\/p>\n

\u758f\u6eb6\u5242\u7406\u8bba\uff1b<\/span> 
<\/span>\u6b63\u76f8<\/span>–<\/span>\u6d41\u52a8\u76f8\u4e0e\u6eb6\u8d28\u6392\u65a5\u529b\u5f3a\uff0c\u4f5c\u7528\u65f6\u95f4<\/span>\u2191<\/span>\uff0c<\/span>K\u2191<\/span>\uff0c\u7ec4\u5206<\/span>tR<\/sub>\u2191<\/span>\uff1b<\/span>
<\/span>\u53cd\u76f8<\/span>–<\/span>\u6d41\u52a8\u76f8\u4e0e\u6eb6\u8d28\u6392\u65a5\u529b\u5f31\uff0c\u4f5c\u7528\u65f6\u95f4<\/span>\u2193<\/span>\uff0c<\/span>K\u2193<\/span>\uff0c\u7ec4\u5206<\/span>tR<\/sub>\u2193<\/span>\uff1b<\/span>
<\/span>\uff082\uff09<\/span>\u56fa\u5b9a\u76f8\uff1a<\/span><\/strong><\/span><\/p>\n

\u6781\u6027\u5c0f\u7684\u70f7\u57fa\u952e\u5408\u76f8\uff1b<\/span>
C8<\/sub><\/span>\u67f1\uff0c<\/span>C18<\/sub><\/span>\u67f1\uff08<\/span>ODS<\/span>\u67f1<\/span>-HPLC<\/span>\u7ea6<\/span>80%<\/span>\u95ee\u9898\uff09\uff1b<\/span>
<\/span>\uff083\uff09<\/span>\u6d41\u52a8\u76f8\uff1a<\/span><\/strong><\/span><\/p>\n

\u6781\u6027\u5927\u7684\u7532\u9187<\/span>–<\/span>\u6c34\u6216\u4e59\u8148<\/span>–<\/span>\u6c34\uff1b<\/span>
<\/span>\u6d41\u52a8\u76f8\u6781\u6027<\/span>><\/span>\u56fa\u5b9a\u76f8\u6781\u6027\uff1b<\/span>
<\/span>\u5e95\u5242<\/span>+<\/span>\u6709\u673a\u8c03\u8282\u5242\uff08\u6781\u6027\u8c03\u8282\u5242\uff09\uff1b<\/span>
<\/span>\u4f8b\uff1a\u6c34<\/span>+<\/span>\u7532\u9187\uff0c\u4e59\u8148\uff0c<\/span>THF<\/span>\uff1b<\/span>
<\/span>\uff084\uff09<\/span>\u6d41\u52a8\u76f8\u6781\u6027\u4e0e<\/span>k<\/span>\u7684\u5173\u7cfb\uff1a<\/span><\/strong><\/span><\/p>\n

\u6d41\u52a8\u76f8\u6781\u6027<\/span>\u2191<\/span>\uff0c\u6d17\u8131\u80fd\u529b<\/span>\u2193<\/span>\uff0c<\/span>k\u2191<\/span>\uff0c\u7ec4\u5206<\/span>tR<\/sub>\u2191
<\/span>\uff085\uff09<\/span>\u51fa\u67f1\u987a\u5e8f\uff1a<\/span><\/strong><\/span><\/p>\n

\u6781\u6027\u5927\u7684\u7ec4\u5206\u5148\u51fa\u67f1\uff1b<\/span><\/p>\n

\u6781\u6027\u5c0f\u7684\u7ec4\u5206\u540e\u51fa\u67f1\uff1b<\/span>
<\/span>\uff086\uff09<\/span>\u9002\u7528\uff1a<\/span><\/strong><\/span><\/p>\n

\u975e\u6781\u6027<\/span>~<\/span>\u4e2d\u7b49\u6781\u6027\u7ec4\u5206\uff08<\/span>HPLC 80%<\/span>\u95ee\u9898\uff09<\/span><\/span><\/p>\n

3.<\/span>\u6b63\u76f8\u952e\u5408\u76f8\u8272\u8c31<\/span><\/span><\/strong><\/span>
<\/span>(1)\u5206\u79bb\u673a\u5236\uff1a<\/span><\/strong><\/span><\/p>\n

\u6eb6\u8d28\u5206\u5b50\u4e0e\u56fa\u5b9a\u76f8\u4e4b\u95f4\u5b9a\u5411\u4f5c\u7528\u529b\u3001\u8bf1\u5bfc\u529b\u3001\u6216\u6c22\u952e\u4f5c\u7528\u529b<\/span>
<\/span>(2)\u56fa\u5b9a\u76f8\uff1a<\/span><\/strong><\/span><\/p>\n

\u6781\u6027\u5927\u7684\u6c30\u57fa\u6216\u6c28\u57fa\u952e\u5408\u76f8\uff1b<\/span>
<\/span>(3)\u6d41\u52a8\u76f8\uff1a<\/span><\/strong><\/span><\/p>\n

\u6781\u6027\u5c0f\uff08\u540c<\/span>LSC<\/span>\uff09\uff1b\u5e95\u5242<\/span>+<\/span>\u6709\u673a\u6781\u6027\u8c03\u8282\u5242\uff1b<\/span> 
<\/span>\u4f8b\uff1a<\/span><\/strong>\u6b63\u5df1\u70f7<\/span>+<\/span>\u6c2f\u4eff<\/span>–<\/span>\u7532\u9187\uff0c\u6c2f\u4eff<\/span>–<\/span>\u4e59\u9187\uff1b<\/span>
<\/span>(4)\u6d41\u52a8\u76f8\u6781\u6027\u4e0e<\/span>K<\/span>\u7684\u5173\u7cfb\uff1a<\/span><\/strong>
<\/span>\u6d41\u52a8\u76f8\u6781\u6027<\/span>\u2191<\/span>\uff0c\u6d17\u8131\u80fd\u529b<\/span>\u2191<\/span>\uff0c\u7ec4\u5206<\/span>tR<\/sub>\u2193<\/span>\uff0c<\/span>k\u2193<\/span>\uff1b<\/span>
<\/span>(5)\u51fa\u67f1\u987a\u5e8f\uff1a<\/span><\/strong><\/span><\/p>\n

\u7ed3\u6784\u76f8\u8fd1\u7ec4\u5206\uff0c\u6781\u6027\u5c0f\u7684\u7ec4\u5206\u5148\u51fa\u67f1\uff0c\u6781\u6027\u5927\u7684\u7ec4\u5206\u540e\u51fa\u67f1\uff1b<\/span>
<\/span>(6)\u9002\u7528\uff1a<\/span><\/strong>
<\/span>\u6c30\u57fa\u952e\u5408\u76f8\u4e0e\u7845\u80f6\u7684\u67f1\u9009\u62e9\u6027\u76f8\u4f3c\uff08\u6781\u6027\u7a0d\u5c0f\uff09\uff0c\u5206\u79bb\u7269\u8d28\u4e5f\u76f8\u4f3c\uff1b<\/span>
<\/span>\u6c28\u57fa\u952e\u5408\u76f8\u4e0e\u7845\u80f6\u6027\u8d28\u5dee\u522b\u5927\uff0c\u78b1\u6027\uff0c\u5206\u6790\u6781\u6027\u5927\u7269\u8d28\u3001\u7cd6\u7c7b\u7b49\uff1b<\/span>
<\/span>4.\u79bb\u5b50\u5bf9\u8272\u8c31\u548c\u79bb\u5b50\u6291\u5236\u8272\u8c31<\/span><\/strong>
<\/span>\u53cd\u76f8\u79bb\u5b50\u5bf9\u8272\u8c31\u6cd5\uff08<\/span>IPC<\/span>\u6216<\/span>PIC<\/span>\uff09<\/span> 
<\/span>\u53cd\u76f8\u8272\u8c31\u4e2d\uff0c\u5728\u6781\u6027\u6d41\u52a8\u76f8\u4e2d\u52a0\u5165\u79bb\u5b50\u5bf9\u8bd5\u5242\uff0c\u4f7f\u88ab\u6d4b\u7ec4\u5206\u4e0e\u5176\u4e2d\u7684\u53cd\u79bb\u5b50\u5f62\u6210\u4e2d\u6027\u79bb\u5b50\u5bf9\uff0c\u589e\u52a0<\/span>K<\/span>\u548c<\/span>tR<\/sub><\/span>\uff0c\u4ee5\u6539\u5584\u5206\u79bb\uff1b<\/span>
<\/span>(1)<\/span>\u79bb\u5b50\u5bf9\u8bd5\u5242\uff1a<\/span><\/strong><\/span><\/p>\n

\u70f7\u57fa\u78fa\u9178\u94a0<\/span>\u2192<\/span>\u5206\u6790\u78b1<\/span>
<\/span>\u56db\u4e01\u57fa\u5b63\u80fa\u76d0<\/span>\u2192<\/span>\u5206\u6790\u9178<\/span>
<\/span>(2)<\/span>\u5f71\u54cd<\/span>K<\/span>\u7684\u56e0\u7d20:<\/span><\/strong>
a<\/span>\uff0e\u4e0e<\/span>m<\/span>\u7684\u6781\u6027\u6709\u5173\uff08\u540c\u53cd\u76f8\u8272\u8c31\uff09\uff1b<\/span>
b<\/span>\uff0e\u4e0e<\/span>R<\/span>\u7684\u94fe\u957f\u6709\u5173\uff1a<\/span>R\u2191<\/span>\u957f\uff0c\u6781\u6027<\/span>\u2193<\/span>\u5c0f\uff0c<\/span>tR<\/sub>\u2191<\/span>\uff0c<\/span>k\u2191<\/span>\uff1b<\/span>
<\/span>(3)<\/span>\u9002\u7528\uff1a<\/span><\/strong><\/span><\/p>\n

\u8f83\u5f3a\u7684\u6709\u673a\u9178\u3001\u78b1\uff1b<\/span><\/p>\n

\u53cd\u76f8\u79bb\u5b50\u6291\u5236\u8272\u8c31\uff1b<\/span>
<\/span>\u5728\u53cd\u76f8\u8272\u8c31\u4e2d\uff0c\u901a\u8fc7\u52a0\u5165\u7f13\u51b2\u6eb6\u6db2\u8c03\u8282\u6d41\u52a8\u76f8<\/span>pH<\/span>\u503c\uff0c\u6291\u5236\uff1b<\/span>
<\/span>\u7ec4\u5206\u89e3\u79bb\uff0c\u589e\u52a0\u5176<\/span>K<\/span>\u548c<\/span>tR<\/sub><\/span>\uff0c\u4ee5\u8fbe\u5230\u6539\u5584\u5206\u79bb\u76ee\u7684\uff1b<\/span>
<\/span>1<\/span>\uff09\u79bb\u5b50\u6291\u5236\u5242\uff1a<\/span><\/strong><\/span><\/p>\n

\u5f31\u9178\u3001\u5f31\u78b1\u6027\u7269\u8d28\uff1b<\/span><\/p>\n

 pH<\/span>\u4e00\u5b9a\u7684\u7f13\u51b2\u6eb6\u6db2\uff1b<\/span>
<\/span>2<\/span>\uff09<\/span>K<\/span>\u7684\u5f71\u54cd\u56e0\u7d20\uff1a<\/span><\/strong><\/span><\/p>\n

\u4e0e\u6d41\u52a8\u76f8\u6781\u6027\u6709\u5173\uff0c\u8fd8\u4e0e<\/span>pH<\/span>\u503c\u6709\u5173\uff1b<\/span>
<\/span>\u9009\u62e9\u6d41\u52a8\u76f8\uff1a<\/span><\/strong><\/span><\/p>\n

\u5e94\u540c\u65f6\u8003\u8651\u6781\u6027\u53ca<\/span>pH<\/span>\u503c\uff1b<\/span> 
<\/span>\u9178\u6027\u7269\u8d28<\/span>–<\/span>\u52a0\u5165\u9178<\/span>HAc<\/sub><\/span>\uff0c<\/span>tR<\/sub>\u2191<\/span>\uff0c<\/span>K\u2191<\/span>\uff1b<\/span> 
<\/span>\u78b1\u6027\u7269\u8d28<\/span>–<\/span>\u52a0\u5165\u78b1<\/span>NH3<\/sub>\u00b7H2<\/sub>O<\/span>\uff0c<\/span>tR<\/sub>\u2191<\/span>\uff0c<\/span>K\u2191<\/span>\uff1b<\/span>  
<\/span>\u8c03\u8282<\/span>pH<\/span>\u8303\u56f4\uff1a<\/span><\/strong><\/span><\/p>\n

3.0~8.0\uff1b
pH>8.0<\/span>\u7834\u574f\u952e\u5408\u76f8\u4e0e\u8f7d\u4f53\u7684\u7ed3\u5408\uff1b<\/span>
pH<3.0<\/span>\u8150\u8680\u67f1\u5b50\uff1b<\/span>
<\/span>3<\/span>\uff09\u9002\u7528\uff1a<\/span><\/strong><\/span><\/p>\n

\u6781\u5f31\u9178\u78b1\u7269\u8d28\uff1b<\/span>
pH=3~7<\/span>\u5f31\u9178\uff1b<\/span><\/span><\/p>\n

pH=7~8<\/span>\u5f31\u78b1\uff1b<\/span><\/span><\/p>\n

\u4e24\u6027\u5316\u5408\u7269\uff1b<\/span><\/p>\n

\u672c\u6587\u8f6c\u81ea\u836f\u7269\u5206\u6790\u4e4b\u5bb6<\/p>\n

\u8fd1\u671f\u57f9\u8bad<\/span><\/p>\n


<\/p>\n

\n
\n
\n
\n
\u8fd1\u70ed\u95e8\u57f9\u8bad\u8bfe\u7a0b<\/strong><\/span>\u671f<\/strong>\u8bf7\u70b9\u51fb\u4e0b\u9762<\/strong><\/span>\u84dd\u8272\u8bfe<\/strong><\/span>\u539f<\/strong>\u9898\u94fe\u63a5<\/strong><\/span>\u9605\u8bfb<\/strong>\u6587

<\/strong><\/span><\/p>
\u6210\u90fd\u5e028 \u670824- 26\u65e5<\/span><\/span>-2018 QA\u4e13\u5458\u6280\u80fd\u5b8c\u5584\u3001\u63d0\u5347\u4e0e\u5b9e\u64cd\u4e13\u9898\u57f9\u8bad\u73ed<\/span>\u201d\u7684\u901a\u77e5<\/span><\/span><\/strong><\/a>

<\/span><\/strong><\/strong><\/span><\/p>
\u6b66\u6c49<\/span>8<\/span>\u6708<\/span>31-9<\/span>\u6708<\/span>2<\/span>\u65e5<\/span><\/strong><\/span><\/a>-\u836f\u54c1\u5236\u5907\u5de5\u827a\u5f00\u53d1\u4e0e\u5de5\u827a\u9a8c\u8bc1<\/span>\/\u6301\u7eed\u5de5\u827a\u786e\u8ba4\u7814\u7a76\u4e0e\u5b9e\u65bd\u201d\u7b2c\u56db\u671f\u7814\u4fee\u73ed\u7684\u901a\u77e5<\/span><\/strong><\/span><\/a>

<\/span><\/strong><\/p>
\u5317\u4eac<\/span>9\u670813-15\u65e5<\/span>-2018\u836f\u4f01OOS\/OOT\u8c03\u67e5\u8bef\u533a\u4e0e\u6539\u8fdb\u5b9e\u64cd \u4e13\u9898\u57f9\u8bad\u73ed\u201d\u7684\u901a\u77e5<\/span><\/strong><\/a><\/p>
<\/span><\/strong>
<\/p>
\u4e0a\u6d77<\/span><\/strong><\/strong><\/span><\/p>

<\/p>
\u4e0a\u6d77\u5e028\u670817-19\u65e5<\/span><\/span>-<\/span>\u65e0\u83cc\u751f\u4ea7\u5982\u4f55\u901a\u8fc7\u56fd\u5185\u5916<\/span>cGMP<\/span>\u8ba4\u8bc1<\/span>\u201d<\/span><\/a>\u4e13\u9898\u57f9\u8bad\u73ed\u7684\u901a\u77e5

<\/a>\u4e0a\u6d778\u67089\u65e5-11\u65e5<\/span>-\u836f\u54c1\u751f\u4ea7\u5de5\u827a\u53d8\u66f4\u7814\u7a76\u53ca\u5de5\u827a\u53d8\u66f4\u9a8c\u8bc1\u5b9e\u65bd\u4e13\u9898\u7814\u4fee\u73ed\u7684\u901a\u77e5<\/span><\/a>

<\/strong><\/span><\/span><\/span><\/strong><\/strong><\/span><\/p><\/section>
\u4e0a\u6d77-<\/span>9\u670814-16\u65e5<\/span>\u7b26\u5408GMP\u7684\u5236\u836f\u5de5\u7a0b\u9879\u76ee\u7ba1\u7406\u548c\u8bbe\u65bd\u8c03\u8bd5\u4e0e\u786e\u8ba4\u5b9e\u65bd
\u201d\u7814\u4fee\u73ed<\/span><\/strong><\/span>

\u5357\u4eac<\/span><\/strong>
<\/p>
<\/span><\/a><\/span><\/strong><\/span>\u82cf\u5dde9\u670813-15\u65e5<\/span><\/span>-\u836f\u4f01\u5b9e\u9a8c\u5ba4\uff08\u7814\u53d1<\/span>\/QC\uff09\u89c4\u8303\u7ba1\u7406\u4e0e<\/span>ICH\u6307\u5357\u53ca\u836f\u5178\u6700\u65b0\u8fdb\u5c55<\/span><\/a>
<\/span><\/strong>
<\/span><\/strong><\/span>\u5357\u4eac\u5e02\u6708<\/a><\/span><\/strong>9<\/a>\u6708<\/span><\/strong><\/span>5-7\u65e5<\/span>-<\/span>\u65b0\u836f\u7814\u53d1\u9879\u76ee\u7b5b\u9009\u4e0e\u7acb\u9879\u53ca\u7efc\u5408\u4fe1\u606f\u6316\u6398\u5b9e\u6218\u5206\u6790\u201d\u4e13\u9898\u57f9\u8bad\u73ed\u901a\u77e5<\/span><\/strong><\/a><\/p>

<\/p>
\u5357\u4eac\u5e029\u670813\u65e5-15\u65e5<\/span><\/span>-\u7b2c\u4e8c\u671f\u7ed3\u6676\u5de5\u827a\u5f00\u53d1\u7814\u7a76\u548c\u8bbe\u8ba1\u57f9\u8bad\u73ed<\/span><\/span><\/strong><\/span><\/a>
<\/span><\/strong><\/span><\/p>
<\/strong><\/span><\/strong><\/strong>
<\/span><\/p>
\u5357\u4eac\u5e028\u6708 17 \u65e5\u81f319\u65e5<\/span><\/span>-2018CFDA\u300a\u836f\u54c1\u6570\u636e\u7ba1\u7406\u89c4\u8303\u300b\u89e3\u8bfb\u4e0e\u6848\u4f8b\u89e3\u6790\u9ad8\u7ea7\u57f9\u8bad\u73ed<\/span>\u201d<\/span><\/strong><\/span><\/a>
<\/p>

\u5357\u4eac\u5e029\u670827---9\u670829\u65e5<\/strong>-\u65b0\u6cd5\u89c4\u73af\u5883\u4e0b\u836f\u54c1\u6280\u672f\u8f6c\u79fb\u7b56\u7565\u4e0e\u5b9e\u65bd\u64cd\u4f5c \u9ad8\u7ea7\u57f9\u8bad\u73ed\u7684\u901a\u77e5<\/span><\/strong><\/span><\/a>

<\/p>
\u5c71\u4e1c<\/strong><\/span><\/strong><\/span><\/p>
\uff08\u6d4e\u53578<\/span>\u6708<\/span>26-28<\/span>\u65e5<\/span><\/span>-\u6210\u90fd9<\/span>\u6708<\/span>26-28<\/span>\u65e5<\/span>\uff09\u539f\u6599\u836f\u3001\u836f\u7528\u8f85\u6599\u548c\u836f\u5305\u6750\u5171\u540c\u5ba1\u8bc4\u5ba1\u6279\u89e3\u6790\u53ca\u5982\u4f55\u7f16\u5199\u7533\u62a5\u8d44\u6599\u4e13\u9898\u57f9\u8bad\u73ed\u201d\u7684\u901a\u77e5<\/span><\/strong><\/span><\/a><\/p>
<\/span><\/strong>
<\/span><\/p>
\u9752\u5c9b\u5e02<\/span>-8\u670830---9\u67081\u65e5 <\/span>\u65b0\u6cd5\u89c4\u73af\u5883\u4e0b\u836f\u54c1\u7814\u53d1\u8d28\u91cf\u4f53\u7cfb\u7684\u5efa\u7acb\u4e0e\u5b9e\u65bd\u548c\u64cd\u4f5c\u9ad8\u7ea7\u7ecf\u7406\u4eba\u201d<\/span><\/strong><\/span><\/a>
 <\/span>
<\/span><\/strong><\/span><\/p>
\u6d4e\u5357\u5e028\u670824-26\u65e5<\/span><\/span>-2018 \u786e\u8ba4\u4e0e\u9a8c\u8bc1\u4e13\u5458\u6280\u80fd\u5f3a\u5316\u4e13\u9898\u57f9\u8bad\u73ed\u7684\u901a\u77e5<\/span><\/span><\/strong><\/span><\/a>
<\/p>
\u676d\u5dde<\/strong><\/span><\/p>
\u676d\u5dde8\u670810\u65e5-8\u670812\u65e5<\/span><\/span>-2018\u836f\u4f01\u504f\u5dee\u4e0e\u53d8\u66f4\u5b9e\u65bd\u4e0e\u6539\u8fdb \u4e13\u9898\u57f9\u8bad\u73ed<\/span>\u201d\u7684\u901a\u77e5<\/span><\/a>

<\/span><\/strong><\/span><\/p>
\uff08\u6c88\u96338<\/span>\u6708<\/span>17-19<\/span>\u65e5<\/span><\/span>-\u676d\u5dde9<\/span>\u6708<\/span>14-16<\/span>\u65e5<\/span>\uff09<\/span>2018\u4f18\u79c0<\/span>GMP\u90e8\u95e8\u7ecf\u7406\u4e1a\u52a1\u53ca\u7ba1\u7406\u80fd\u529b\u63d0\u5347\u9ad8\u7ea7\u7814\u4fee\u73ed\u201d\u7684\u901a\u77e5<\/span><\/strong><\/span><\/a><\/p>


<\/span><\/strong>\u676d\u5dde<\/span>-<\/span>8\u670824-26\u65e5<\/span>\u4e34\u5e8a\u8bd5\u9a8c\u7528\u836f<\/span>GMP<\/span>\u5236\u5ea6\u8981\u70b9\u89e3\u6790\u53ca\u5e94\u7528\u5b9e\u65bd\u4e13\u9898\u57f9\u8bad\u73ed\u201d\u7684\u901a\u77e5<\/span><\/a><\/span><\/strong><\/span><\/span><\/p>

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\u5929\u6d25\u5e02<\/span>9\u67082\u65e5-9\u67084\u65e5<\/span>-\u65b0\u6cd5\u89c4\u80cc\u666f\u4e0b\u4fdd\u5065\u98df\u54c1\u914d\u65b9\u8bbe\u8ba1\u3001\u914d\u65b9\u4f9d\u636e\u4e0e\u6280\u672f\u8981\u6c42\u5236\u5b9a\u5b9e\u6218\u66a8\u7ecf\u5178\u6848\u4f8b\u5206\u4eab\u54a8\u8be2\u4f1a\u201d\u7684\u901a\u77e5<\/span><\/a><\/strong><\/p><\/section><\/pre>\n

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\u7ec4\u56e2\u62a5\u540d<\/span><\/strong>\u627e\u5c1a\u8001\u5e08\u4eab<\/span>\u4f18\u60e0\u66f4\u5927\u3002<\/span><\/span><\/strong><\/a><\/span><\/strong><\/span><\/p><\/pre>\n<\/section>\n
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