{"id":81834,"date":"2019-02-27T00:00:50","date_gmt":"2019-04-11T06:54:01","guid":{"rendered":"http:\/\/www.05921.net\/index.php\/81834\/"},"modified":"2019-04-11T14:54:01","modified_gmt":"2019-04-11T06:54:01","slug":"0c07353ddb","status":"publish","type":"post","link":"https:\/\/www.05921.net\/index.php\/81834\/","title":{"rendered":"\u3010\u6536\u85cf\u30119\u79cd\u6700\u5e38\u89c1\u7684\u836f\u7269\u6676\u578b\u68c0\u6d4b\u65b9\u6cd5"},"content":{"rendered":"
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X-\u5c04\u7ebf\u884d\u5c04\u6cd5\uff08X-ray diffraction\uff09<\/strong><\/span><\/section>\n<\/section>\n
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X-\u5c04\u7ebf\u884d\u5c04\u662f\u7814\u7a76\u836f\u7269\u6676\u578b\u7684\u4e3b\u8981\u624b\u6bb5\uff0c\u8be5\u65b9\u6cd5\u53ef\u7528\u4e8e\u533a\u522b<\/span>\u6676\u6001\u548c\u975e\u6676\u6001<\/span>\uff0c\u9274\u522b\u6676\u4f53\u7684\u54c1\u79cd\uff0c\u533a\u522b\u6df7\u5408\u7269\u548c\u5316\u5408\u7269\uff0c\u6d4b\u5b9a\u836f\u7269\u6676\u578b\u7ed3\u6784\uff0c\u6d4b\u5b9a\u6676\u80de\u53c2\u6570\uff08\u5982\u539f\u5b50\u95f4\u7684\u8ddd\u79bb\u3001\u73af\u5e73\u9762\u7684\u8ddd\u79bb\u3001\u53cc\u9762\u5939\u89d2\u7b49\uff09\uff0c\u8fd8\u53ef\u7528\u4e8e\u4e0d\u540c\u6676\u578b\u7684\u6bd4\u8f83\u3002X-\u5c04\u7ebf\u884d\u5c04\u6cd5\u53c8\u5206\u4e3a\u7c89\u672b\u884d\u5c04\u548c\u5355\u6676\u884d\u5c04\u4e24\u79cd\uff0c\u524d\u8005\u4e3b\u8981\u7528\u4e8e\u7ed3\u6676\u7269\u8d28\u7684<\/span>\u9274\u522b<\/strong><\/span>\u53ca<\/span>\u7eaf\u5ea6\u68c0\u67e5<\/span><\/strong>\uff0c\u540e\u8005\u4e3b\u8981\u7528\u4e8e<\/span>\u5206\u5b50\u91cf<\/span><\/strong>\u548c<\/span>\u6676\u4f53\u7ed3\u6784<\/span><\/strong>\u7684\u6d4b\u5b9a\u3002<\/span><\/span><\/p>\n

 \u3000<\/mpcpc><\/span><\/p>\n

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\u3000<\/span><\/p>\n

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<\/p>\n

\u7ea2\u5916\u5149\u8c31\u6cd5\u5e38\u7528\u7684\u6837\u54c1\u5236\u5907\u65b9\u6cd5\u6709KBr\u538b\u7247\u6cd5\u3001\u77f3\u8721\u7cca\u6cd5\u3001\u6f2b\u53cd\u5c04\u6cd5\u4ee5\u53ca\u8870\u51cf\u5168\u53cd\u5c04\u6cd5\uff08attenuated total reflection, ATR\uff09\u7b49\u3002\u8003\u8651\u5230\u7814\u78e8\u53ef\u80fd\u4f1a\u5bfc\u81f4\u836f\u7269\u6676\u578b\u7684\u6539\u53d8\uff0c\u6240\u4ee5\u5728\u7528\u7ea2\u5916\u5149\u8c31\u6cd5\u8fdb\u884c\u836f\u7269\u6676\u578b\u6d4b\u5b9a\u65f6\u591a\u91c7\u7528<\/span>\u77f3\u8721\u6cb9\u7cca\u6cd5<\/strong><\/span>\uff0c\u6216\u91c7\u7528<\/span>\u6269\u6563\u53cd\u5c04\u7ea2\u5916\u5085\u91cc\u53f6\u53d8\u5316\u5149\u8c31\u6cd5<\/strong><\/span>\uff08DRIFT\uff09\u3002<\/span><\/span><\/p>\n


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\u3000<\/mpcpc><\/span><\/p>\n

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<\/p>\n

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\u3000\u3000<\/span>\u3000<\/span><\/p>\n

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\u3000<\/span><\/p>\n

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\u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\uff08differential scanning calorimeter, DSC\uff09<\/span><\/section>\n<\/section>\n<\/section>\n<\/section>\n

DSC\u662f\u5728\u7a0b\u5e8f\u63a7\u5236\u4e0b\uff0c\u901a\u8fc7\u4e0d\u65ad\u52a0\u70ed\u6216\u964d\u6e29\uff0c\u6d4b\u91cf\u6837\u54c1\u4e0e\u60f0\u6027\u53c2\u6bd4\u7269\uff08\u5e38\u7528\u03b1-Al2O3\uff09\u4e4b\u95f4\u7684<\/span>\u80fd\u91cf\u5dee<\/strong><\/span>\u968f\u6e29\u5ea6\u53d8\u5316\u7684\u4e00\u79cd\u6280\u672f\u3002DSC\u591a\u7528\u4e8e\u5206\u6790\u6837\u54c1\u7684\u7194\u878d\u5206\u89e3\u60c5\u51b5\u4ee5\u53ca\u662f\u5426\u6709\u8f6c\u6676\u6216\u6df7\u6676\u73b0\u8c61\u3002<\/span><\/span><\/p>\n

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\u5dee\u70ed\u5206\u6790\u6cd5\uff08differential thermal analysis, DTA\uff09<\/span><\/section>\n<\/section>\n
DTA\u548cDSC\u8f83\u4e3a\u76f8\u4f3c\uff0c\u6240\u4e0d\u540c\u7684\u662f\uff0cDTA\u662f\u901a\u8fc7\u540c\u6b65\u6d4b\u91cf\u6837\u54c1\u4e0e\u60f0\u6027\u53c2\u6bd4\u7269\u7684\u6e29\u5ea6\u5dee\u6765\u5224\u5b9a\u7269\u8d28\u7684\u5185\u5728\u53d8\u5316\u3002\u5404\u79cd\u7269\u8d28\u90fd\u6709\u81ea\u5df1\u7684\u5dee\u70ed\u66f2\u7ebf\uff0c\u56e0\u6b64DTA\u662f\u7269\u8d28\u7269\u7406\u7279\u6027\u5206\u6790\u7684\u4e00\u79cd\u91cd\u8981\u624b\u6bb5\u3002\u3000\u3000<\/span><\/section>\n
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\u70ed\u91cd\u5206\u6790\u6cd5\uff08thermogravimetric analysis, TGA\uff09<\/span><\/section>\n<\/section>\n<\/section>\n<\/section>\n

TGA\u662f\u5728\u7a0b\u5e8f\u63a7\u5236\u4e0b\uff0c\u6d4b\u5b9a\u7269\u8d28\u7684<\/span>\u8d28\u91cf\u968f\u6e29\u5ea6\u53d8\u5316<\/strong><\/span>\u7684\u4e00\u79cd\u6280\u672f\uff0c\u9002\u7528\u4e8e\u68c0\u67e5\u6676\u4f53\u4e2d\u6eb6\u5242\u7684\u4e27\u5931\u6216\u6837\u54c1\u5347\u534e\u3001\u5206\u89e3\u7684\u8fc7\u7a0b\uff0c\u53ef\u63a8\u6d4b\u6676\u4f53\u4e2d<\/span>\u542b\u7ed3\u6676\u6c34<\/strong><\/span>\u6216<\/span>\u7ed3\u6676\u6eb6\u5242<\/strong><\/span>\u7684\u60c5\u51b5\uff0c\u4ece\u800c\u53ef\u5feb\u901f\u533a\u5206\u65e0\u6c34\u6676\u578b\u4e0e\u5047\u591a\u6676\u578b\u3002\u70ed\u5206\u6790\u6cd5\u6240\u9700\u6837\u54c1\u91cf\u5c11\uff0c\u65b9\u6cd5\u7b80\u4fbf\uff0c\u7075\u654f\u5ea6\u9ad8\uff0c\u91cd\u73b0\u6027\u597d\uff0c\u5728\u836f\u7269\u591a\u6676\u578b\u5206\u6790\u4e2d\u8f83\u4e3a\u5e38\u7528\u3002\u3000\u3000<\/span><\/span>
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\u900f\u660e\u56fa\u4f53\u836f\u7269\u7684\u89c2\u6d4b\u4e00\u822c\u662f\u5728\u6b63\u4ea4\u504f\u5149\u4e0b\u8fdb\u884c\u3002\u7531\u4e8e\u6676\u4f53\u7ed3\u6784\u4e0d\u540c\u548c\u504f\u5149\u5c04\u5165\u65f6\u7684\u53cc\u6298\u5c04\u4f5c\u7528\uff0c\u5728\u504f\u5149\u663e\u5fae\u955c\u4e0a\u3001\u4e0b\u504f\u5149\u955c\u7684\u6b63\u4ea4\u4f5c\u7528\u4e0b\uff0c\u6676\u4f53\u6837\u54c1\u7f6e\u4e8e\u8f7d\u7269\u53f0\u4e0a\u65cb\u8f6c360\u65f6\uff0c\u5219\u6676\u4f53\u663e\u73b0\u77ed\u6682\u7684\u9690\u5931\u548c\u95ea\u4eae\uff0c\u6676\u4f53\u9690\u5931\u65f6\u6676\u4f53\u4e0e\u504f\u632f\u5668\u632f\u52a8\u529b\u5411\u6240\u6210\u7684\u4ea4\u89d2\u79f0\u4e3a\u6d88\u5149\u89d2\uff0c\u901a\u8fc7\u4e0d\u540c\u7684\u6d88\u5149\u89d2\uff0c\u5373\u53ef\u51b3\u5b9a\u6676\u4f53\u6240\u5c5e\u7684\u6676\u578b\u3002\u504f\u5149\u663e\u5fae\u955c\u6cd5\u8fd8\u53ef\u7814\u7a76\u6676\u578b\u95f4\u7684\u76f8\u53d8\uff0c\u53ef\u4ee5\u51c6\u786e\u6d4b\u5b9a\u6676\u4f53\u7194\u70b9\uff1b\u5bf9\u4e8e\u5177\u6709\u5404\u9879\u5411\u5f02\u6027\u7684\u52a8\u690d\u7269\u6750\u6599(\u5982\u7ea4\u7ef4\u86cb\u767d\u3001\u6dc0\u7c89\u7c92)\u7684\u7ed3\u6784\uff0c\u5177\u6709\u7279\u6b8a\u7684\u9274\u5b9a\u4f5c\u7528\u3002\u3000<\/span><\/p>\n

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\u5c24\u5176\u662f\u8fd1\u5e74\u6765\u51fa\u73b0\u7684\u56fa\u600113C\u2014NMR\u3001\u9ad8\u6548\u8d28\u5b50\u53bb\u8026\u5408\u3001\u4ea4\u53c9\u6781\u5316(CP)\u3001\u5e7b\u89d2\u81ea\u65cb(CAS)\u7b49\u65b0\u6280\u672f\u7684\u5e94\u7528\uff0c\u4f7f\u5f97\u6211\u4eec\u80fd\u83b7\u5f97\u9ad8\u5206\u8fa8\u7387\u768413C\u2014NMR\u8c31\uff0c\u8fd9\u79cd\u8c31\u56fe\u80fd\u7ed9\u51fa\u6709\u5173<\/span>\u52a8\u529b\u5b66<\/span><\/strong>\u548c<\/span>\u5c40\u90e8\u5316\u5b66\u73af\u5883<\/span><\/strong>\u7684\u8be6\u7ec6\u539f\u5b50\u6c34\u5e73\u7684\u4fe1\u606f\uff0c\u56e0\u6b64\u5229\u8fd9\u79cd\u9ad8\u5206\u8fa8\u7387\u768413C\u2014NMR\u8c31\u56fe\u53ef\u8fdb\u884c<\/span>\u591a\u6676\u578b\u7684\u6df7\u6676\u5206\u6790<\/span><\/strong>\u4ee5\u53ca\u67d0\u79cd\u7279\u5f81\u6676\u578b\u7684\u6d4b\u5b9a\u3002\u3000\u3000<\/span><\/span><\/p>\n

\u3000<\/span><\/p>\n

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\n<\/section>\n<\/section>\n<\/section>\n

\u3000\u3000<\/span>
<\/p>\n

\u4e0a\u8ff0\u6240\u63d0\u53ca\u7684\u836f\u7269\u6676\u578b\u786e\u5b9a\u65b9\u6cd5\u591a\u6570\u4ec5\u80fd\u53cd\u6620\u836f\u7269\u4e0d\u540c\u6676\u578b\u67d0\u4e00\u65b9\u9762\u7684\u7269\u7406\u6027\u8d28\uff0c\u56e0\u6b64\uff0c\u4e0d\u540c\u6d4b\u8bd5\u624b\u6bb5\u7684\u7efc\u5408\u8fd0\u7528\uff0c\u53ef\u8fbe\u5230\u5bf9\u836f\u7269\u6676\u578b\u7684\u5168\u9762\u8ba4\u8bc6\u3002\u8fd1\u5e74\u6765\u51fa\u73b0\u7684\u7ea2\u5916\u4e0e\u70ed\u663e\u5fae\u955c\u6cd5\uff0c\u4ee5\u53ca\u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\u4e0e\u70ed\u53f0\u663e\u5fae\u955c\u6cd5\u8054\u7528\u65b9\u6cd5\u5373\u662f\u8be5\u601d\u8def\u7684\u4e00\u79cd\u4f53\u73b0\u3002<\/span><\/p>\n


<\/p>\n

————THE END————<\/span><\/p>\n


<\/p>\n

\u5185\u5bb9<\/span><\/em>\u6765\u6e90\uff1a\u5b9e\u9a8c\u4e0e\u5206\u6790\uff0c<\/span><\/em>\u7f16\u8f91\u6574\u7406<\/span><\/em><\/p>\n

<\/mpcps><\/section>\n


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